C₃₅H₅₀O₆Si

Base Information

Chemical Name:C₃₅H₅₀O₆Si
CAS No.:1268455-81-7
Molecular Formula:C₃₅H₅₀O₆Si
Molecular Weight:594.864
Hs Code.:

C<sub>35</sub>H<sub>50</sub>O<sub>6</sub>Si

Synonyms:C₃₅H₅₀O₆Si

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Chemical Property of C₃₅H₅₀O₆Si

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Technology Process of C₃₅H₅₀O₆Si

There total 23 articles about C₃₅H₅₀O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1268455-43-1
C₂₈H₃₈O₄SSi

: 1268455-41-9
C₁₇H₂₈O₂Sn

: 1268455-81-7
C₃₅H₅₀O₆Si

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; ((diphenylphosphoryl)oxy)copper(I); triphenyl-arsane; In tetrahydrofuran; at 20 ℃; for 1.5h;
DOI:10.1246/bcsj.20120152

Reference yield:

: C₁₅H₁₉F₃O₅S

: 1268455-43-1
C₂₈H₃₈O₄SSi

: 1268455-81-7
C₃₅H₅₀O₆Si

Guidance literature:: C₁₅H₁₉F₃O₅S; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; hexamethyldistannane; lithium chloride; In tetrahydrofuran; at 70 ℃; for 1.5h;

C₂₈H₃₈O₄SSi; With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; ((diphenylphosphoryl)oxy)copper(I); triphenyl-arsane; In tetrahydrofuran; at 20 ℃; for 3.5h;
DOI:10.1021/ol1031409

Reference yield:

: 1268455-52-2
C₂₄H₃₈O₄Si

: 1268455-81-7
C₃₅H₅₀O₆Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

2.2: 0 - 20 °C

3.1: methanol; camphor-10-sulfonic acid / dichloromethane / 12 h / 20 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 14.5 h / 50 °C

5.1: methanol; camphor-10-sulfonic acid / dichloromethane / 2 h / 0 °C

6.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 0.5 h / 0 °C

7.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1.5 h / 20 °C

8.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

9.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; hexamethyldistannane; lithium chloride / tetrahydrofuran / 1.5 h / 70 °C

9.2: 3.5 h / 20 °C

With 1H-imidazole; methanol; dmap; sodium chlorite; sodium dihydrogenphosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2-methyl-but-2-ene; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hexamethyldistannane; sulfur trioxide pyridine complex; sodium hydride; triethylamine; dicyclohexyl-carbodiimide; lithium chloride; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; tert-butyl alcohol;
DOI:10.1021/ol1031409