(S)-1-(Methylamino)-2-propanol HCl

Base Information

• Chemical Name: (S)-1-(Methylamino)-2-propanol HCl
• CAS No.: 70377-76-3
• Molecular Formula: C₄H₁₁NO
• Molecular Weight: 89.1374
• Mol file: 70377-76-3.mol

Synonyms:(S)-N-Methyl-2-hydroxypropylamine

Chemical Property of (S)-1-(Methylamino)-2-propanol HCl

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

(S)-1-(Methylamino)-2-propanolHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of (S)-1-(Methylamino)-2-propanol HCl

There total 2 articles about (S)-1-(Methylamino)-2-propanol HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

(S)-ethyl 2-((2-hydroxypropyl)amino)acetate (402723-79-9) → (S)-N-Methyl-2-hydroxypropylamine (70377-76-3)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Reflux;

Reference yield:

(S) lactic acid N-methyl amide (60915-12-0) → (S)-N-Methyl-2-hydroxypropylamine (70377-76-3)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; Heating;

DOI:10.1021/jo01329a025

Reference yield: 70.0%

7-chloro-N-[(1S)-1-cyclopropyl-2,2,2-trifluoroethyl]-6-fluoro-4-oxo-1-(2,4,6-trifluorophenyl)-1,4-dihydro-1,8-naphthyridine-3-carboxamide + (S)-N-Methyl-2-hydroxypropylamine (70377-76-3) → N-[(1S)-1-cyclopropyl-2,2,2-trifluoroethyl]-6-fluoro-7-{[(2S)-2-hydroxypropyl](methyl)amino}-4-oxo-1-(2,4,6-trifluorophenyl)-1,4-dihydro-1,8-naphthyridine-3-carboxamide

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

upstream raw materials:

(S) lactic acid N-methyl amide

(S)-ethyl 2-((2-hydroxypropyl)amino)acetate

Downstream raw materials:

(S)-N-Methyl-N-nitroso-2-hydroxypropylamin

(C₆H₁₁)2POCH(CH₃)CH₂N(CH₃)P(C₅H₉)2

(C₅H₉)2POCH(CH₃)CH₂N(CH₃)P(C₆H₁₁)2

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