(2R,3S)-2-Hydroxy-3-(toluene-4-sulfonylamino)-decanoic acid ethyl ester

Base Information

Chemical Name:(2R,3S)-2-Hydroxy-3-(toluene-4-sulfonylamino)-decanoic acid ethyl ester
CAS No.:181137-45-1
Molecular Formula:C₁₉H₃₁NO₅S
Molecular Weight:385.525
Hs Code.:

Synonyms:(2R,3S)-2-Hydroxy-3-(toluene-4-sulfonylamino)-decanoic acid ethyl ester

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Chemical Property of (2R,3S)-2-Hydroxy-3-(toluene-4-sulfonylamino)-decanoic acid ethyl ester

Chemical Property:

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Technology Process of (2R,3S)-2-Hydroxy-3-(toluene-4-sulfonylamino)-decanoic acid ethyl ester

There total 3 articles about (2R,3S)-2-Hydroxy-3-(toluene-4-sulfonylamino)-decanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 162518-06-1
(R)-4-methyl-N-(5-oxotetrahydrofuran-3-yl)benzenesulfonamide

: 181137-45-1
(2R,3S)-2-Hydroxy-3-(toluene-4-sulfonylamino)-decanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / NaHMDS, 3-phenyl-2-(phenylsulfonyl)oxaziridine / tetrahydrofuran / 2 h / -78 °C

2: 88 percent / Me₃SiI / CH₂Cl₂ / 5.5 h / 20 °C

3: 1.) CuI / 1.) THF, Et₂O, -40 deg C, 2.) THF, -30 deg C, 18 h

With copper(l) iodide; trimethylsilyl iodide; sodium hexamethyldisilazane; N-(benzenesulfonyl)-3-phenyloxaziridine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/hlca.19960790426

Reference yield:

: 162601-64-1
(2R,3S)-2-hydroxy-3-(tosylamino)butano-4-lactone

: 181137-45-1
(2R,3S)-2-Hydroxy-3-(toluene-4-sulfonylamino)-decanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / Me₃SiI / CH₂Cl₂ / 5.5 h / 20 °C

2: 1.) CuI / 1.) THF, Et₂O, -40 deg C, 2.) THF, -30 deg C, 18 h

With copper(l) iodide; trimethylsilyl iodide; In dichloromethane;
DOI:10.1002/hlca.19960790426

Reference yield:

: 21369-64-2
n-hexyllithium

: 162518-07-2
ethyl (2R,3R)-3-<(N-tosyl)amino>-2-hydroxy-4-iodobutyrate

: 181137-45-1
(2R,3S)-2-Hydroxy-3-(toluene-4-sulfonylamino)-decanoic acid ethyl ester

Guidance literature:: With copper(l) iodide; Yield given. Multistep reaction; 1.) THF, Et₂O, -40 deg C, 2.) THF, -30 deg C, 18 h;
DOI:10.1002/hlca.19960790426