1-Benzyloxy-4-((2R,3S,4R,5S,6S)-3,5-bis-benzyloxy-4-dimethylamino-6-methyl-tetrahydro-pyran-2-yl)-10,12-dimethoxy-8-(2-methoxymethoxy-ethyl)-dibenzo[c,h]chromen-6-one

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Chemical Name:1-Benzyloxy-4-((2R,3S,4R,5S,6S)-3,5-bis-benzyloxy-4-dimethylamino-6-methyl-tetrahydro-pyran-2-yl)-10,12-dimethoxy-8-(2-methoxymethoxy-ethyl)-dibenzo[c,h]chromen-6-one
CAS No.:264615-99-8
Molecular Formula:C₅₂H₅₅NO₁₀
Molecular Weight:854.009
Hs Code.:

1-Benzyloxy-4-((2R,3S,4R,5S,6S)-3,5-bis-benzyloxy-4-dimethylamino-6-methyl-tetrahydro-pyran-2-yl)-10,12-dimethoxy-8-(2-methoxymethoxy-ethyl)-dibenzo[c,h]chromen-6-one

Synonyms:1-Benzyloxy-4-((2R,3S,4R,5S,6S)-3,5-bis-benzyloxy-4-dimethylamino-6-methyl-tetrahydro-pyran-2-yl)-10,12-dimethoxy-8-(2-methoxymethoxy-ethyl)-dibenzo[c,h]chromen-6-one

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Chemical Property of 1-Benzyloxy-4-((2R,3S,4R,5S,6S)-3,5-bis-benzyloxy-4-dimethylamino-6-methyl-tetrahydro-pyran-2-yl)-10,12-dimethoxy-8-(2-methoxymethoxy-ethyl)-dibenzo[c,h]chromen-6-one

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Technology Process of 1-Benzyloxy-4-((2R,3S,4R,5S,6S)-3,5-bis-benzyloxy-4-dimethylamino-6-methyl-tetrahydro-pyran-2-yl)-10,12-dimethoxy-8-(2-methoxymethoxy-ethyl)-dibenzo[c,h]chromen-6-one

There total 4 articles about 1-Benzyloxy-4-((2R,3S,4R,5S,6S)-3,5-bis-benzyloxy-4-dimethylamino-6-methyl-tetrahydro-pyran-2-yl)-10,12-dimethoxy-8-(2-methoxymethoxy-ethyl)-dibenzo[c,h]chromen-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 264615-97-6
3-Methoxy-5-(2-methoxymethoxy-ethyl)-2-trifluoromethanesulfonyloxy-benzoic acid 5-benzyloxy-8-((2R,3S,4R,5S,6S)-3,5-bis-benzyloxy-4-dimethylamino-6-methyl-tetrahydro-pyran-2-yl)-4-methoxy-naphthalen-1-yl ester

: 264615-99-8
1-Benzyloxy-4-((2R,3S,4R,5S,6S)-3,5-bis-benzyloxy-4-dimethylamino-6-methyl-tetrahydro-pyran-2-yl)-10,12-dimethoxy-8-(2-methoxymethoxy-ethyl)-dibenzo[c,h]chromen-6-one

Guidance literature:: With palladium diacetate; tributylphosphine; 1,3-bis-(diphenylphosphino)propane; silver carbonate; In N,N-dimethyl-formamide; at 130 ℃; for 0.25h;
DOI:10.1016/S0040-4039(99)02235-2

Reference yield:

: 155351-76-1
3-methoxy-5-<2-(methoxymethoxy)ethyl>-2-<(trifluoromethanesulfonyl)oxy>benzoic acid

: 264615-99-8
1-Benzyloxy-4-((2R,3S,4R,5S,6S)-3,5-bis-benzyloxy-4-dimethylamino-6-methyl-tetrahydro-pyran-2-yl)-10,12-dimethoxy-8-(2-methoxymethoxy-ethyl)-dibenzo[c,h]chromen-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: EDCI; DMAP / CH₂Cl₂ / 2 h

2: 70 percent / Pd(OAc)2; DPPP; Bu₃P / Ag₂CO₃ / dimethylformamide / 0.25 h / 130 °C

With dmap; palladium diacetate; tributylphosphine; 1,3-bis-(diphenylphosphino)propane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; silver carbonate; In dichloromethane; N,N-dimethyl-formamide; 1: Acylation / 2: Cyclization;
DOI:10.1016/S0040-4039(99)02235-2

Reference yield:

: 5-Benzyloxy-8-((2R,3S,4R,5S,6S)-3,5-bis-benzyloxy-4-dimethylamino-6-methyl-tetrahydro-pyran-2-yl)-4-methoxy-naphthalen-1-ol

: 264615-99-8
1-Benzyloxy-4-((2R,3S,4R,5S,6S)-3,5-bis-benzyloxy-4-dimethylamino-6-methyl-tetrahydro-pyran-2-yl)-10,12-dimethoxy-8-(2-methoxymethoxy-ethyl)-dibenzo[c,h]chromen-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: EDCI; DMAP / CH₂Cl₂ / 2 h

2: 70 percent / Pd(OAc)2; DPPP; Bu₃P / Ag₂CO₃ / dimethylformamide / 0.25 h / 130 °C

With dmap; palladium diacetate; tributylphosphine; 1,3-bis-(diphenylphosphino)propane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; silver carbonate; In dichloromethane; N,N-dimethyl-formamide; 1: Acylation / 2: Cyclization;
DOI:10.1016/S0040-4039(99)02235-2