N,N-dimethyl-N-(4'-metoxycarbonylbenzyl)-N-[(-)-8-phenylmenthoyloxycarbonylmethyl]ammonium bromide

Base Information

Chemical Name:N,N-dimethyl-N-(4'-metoxycarbonylbenzyl)-N-[(-)-8-phenylmenthoyloxycarbonylmethyl]ammonium bromide
CAS No.:1004759-64-1
Molecular Formula:Br*C₂₈H₃₇N₂O₂
Molecular Weight:513.518
Hs Code.:

Synonyms:N,N-dimethyl-N-(4'-metoxycarbonylbenzyl)-N-[(-)-8-phenylmenthoyloxycarbonylmethyl]ammonium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-dimethyl-N-(4'-metoxycarbonylbenzyl)-N-[(-)-8-phenylmenthoyloxycarbonylmethyl]ammonium bromide

Chemical Property:

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Technology Process of N,N-dimethyl-N-(4'-metoxycarbonylbenzyl)-N-[(-)-8-phenylmenthoyloxycarbonylmethyl]ammonium bromide

There total 1 articles about N,N-dimethyl-N-(4'-metoxycarbonylbenzyl)-N-[(-)-8-phenylmenthoyloxycarbonylmethyl]ammonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 35525-86-1
4-cyano-N,N-dimethylbenzylamine

: 80595-59-1
bromoacetic acid (-)-8-phenylmenthol ester

: 1004759-64-1
N,N-dimethyl-N-(4'-metoxycarbonylbenzyl)-N-[(-)-8-phenylmenthoyloxycarbonylmethyl]ammonium bromide

Guidance literature:: In acetonitrile; at 20 ℃;
DOI:10.1002/anie.200703832

Reference yield:

: 1004759-64-1
N,N-dimethyl-N-(4'-metoxycarbonylbenzyl)-N-[(-)-8-phenylmenthoyloxycarbonylmethyl]ammonium bromide

: (2R)-2-(5'-cyano-2'-methylphenyl)-2-(dimethylamino)acetic acid (-)-8-phenylmenthol ester

: 1004759-70-9
(2S)-2-(5'-cyano-2'-methylphenyl)-2-(dimethylamino)acetic acid (-)-8-phenylmenthol ester

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at -40 ℃; for 4h; Title compound not separated from byproducts.;
DOI:10.1002/anie.200703832