N-(2-chloroethyl)-N-(2-cyanoethyl)-N',N''-di-p-tolylphosphoric triamide

Base Information

Chemical Name:N-(2-chloroethyl)-N-(2-cyanoethyl)-N',N''-di-p-tolylphosphoric triamide
CAS No.:76081-14-6
Molecular Formula:C₁₉H₂₄ClN₄OP
Molecular Weight:390.853
Hs Code.:

Synonyms:N-(2-chloroethyl)-N-(2-cyanoethyl)-N',N''-di-p-tolylphosphoric triamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-chloroethyl)-N-(2-cyanoethyl)-N',N''-di-p-tolylphosphoric triamide

Chemical Property:

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Technology Process of N-(2-chloroethyl)-N-(2-cyanoethyl)-N',N''-di-p-tolylphosphoric triamide

There total 2 articles about N-(2-chloroethyl)-N-(2-cyanoethyl)-N',N''-di-p-tolylphosphoric triamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 106-49-0,12221-03-3
p-toluidine

: 76081-08-8
N,N-(β-chloroethyl-β-cyanoethyl)amidophosphoryl dichloride

: 76081-14-6
N-(2-chloroethyl)-N-(2-cyanoethyl)-N',N''-di-p-tolylphosphoric triamide

Guidance literature:: With triethylamine; In benzene; at 20 ℃; for 48h;

Reference yield:

: 1072-66-8
1-(2-cyanoethyl)aziridine

: 76081-14-6
N-(2-chloroethyl)-N-(2-cyanoethyl)-N',N''-di-p-tolylphosphoric triamide

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / POCl₃ / benzene / 10 h / 20 °C

2: 82 percent / triethylamine / benzene / 48 h / 20 °C

With triethylamine; trichlorophosphate; In benzene;