7-[(4-methylphenylsulfanyl)methyl]-7,8-dihydro-[1,3]thiazolo[2,3-i]purine

Base Information

• Chemical Name: 7-[(4-methylphenylsulfanyl)methyl]-7,8-dihydro-[1,3]thiazolo[2,3-i]purine
• CAS No.: 1374684-98-6
• Molecular Formula: C₁₅H₁₄N₄S₂
• Molecular Weight: 314.435

Synonyms:7-[(4-methylphenylsulfanyl)methyl]-7,8-dihydro-[1,3]thiazolo[2,3-i]purine

Chemical Property of 7-[(4-methylphenylsulfanyl)methyl]-7,8-dihydro-[1,3]thiazolo[2,3-i]purine

Chemical Property:

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Technology Process of 7-[(4-methylphenylsulfanyl)methyl]-7,8-dihydro-[1,3]thiazolo[2,3-i]purine

There total 2 articles about 7-[(4-methylphenylsulfanyl)methyl]-7,8-dihydro-[1,3]thiazolo[2,3-i]purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

7-[(4-methylphenylsulfanyl)methyl]-7,8-dihydro-[1,3]thiazolo[2,3-i]purin-6-ium perchlorate (1424011-89-1) → 7-[(4-methylphenylsulfanyl)methyl]-7,8-dihydro-[1,3]thiazolo[2,3-i]purine (1374684-98-6)

Guidance literature:

With sodium acetate; In ethanol; at 20 ℃; for 4h;

DOI:10.1134/S1070428013010211

Reference yield:

6-allylsulfanylpurine (5443-88-9) + p-methylbenzenesulfenyl chloride (933-00-6) → 7-[(4-methylphenylsulfanyl)methyl]-7,8-dihydro-[1,3]thiazolo[2,3-i]purine (1374684-98-6)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid; lithium perchlorate / 12 h / 15 - 20 °C

2: sodium acetate / ethanol / 4 h / 20 °C

With sodium acetate; lithium perchlorate; acetic acid; In ethanol;

DOI:10.1134/S1070428013010211

upstream raw materials:

6-allylsulfanylpurine

p-methylbenzenesulfenyl chloride

7-[(4-methylphenylsulfanyl)methyl]-7,8-dihydro-[1,3]thiazolo[2,3-i]purin-6-ium perchlorate

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