Technology Process of C30H46N4O5SSi
There total 12 articles about C30H46N4O5SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide;
In
ethanol; water;
at 0 - 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1002/anie.201206560
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: toluene / 17 h / 0 - 20 °C / Inert atmosphere
2.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.33 h / -78 °C / Inert atmosphere
2.2: 0.5 h / -78 - 20 °C / Inert atmosphere
3.1: (-)-diisopinocamphenylborane chloride / tetrahydrofuran / 2.33 h / -30 - 20 °C / Inert atmosphere
4.1: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere
5.1: camphor-10-sulfonic acid / dichloromethane; methanol / 0.5 h / 0 °C / Inert atmosphere
6.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 1 h / 0 - 20 °C / Inert atmosphere
7.1: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / water; ethanol / 2 h / 0 - 20 °C / Inert atmosphere
With
2,6-dimethylpyridine; oxalyl dichloride; hexaammonium heptamolybdate tetrahydrate; camphor-10-sulfonic acid; dihydrogen peroxide; dimethyl sulfoxide; triphenylphosphine; (-)-diisopinocamphenylborane chloride; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene;
6.1: |Mitsunobu Displacement;
DOI:10.1002/anie.201206560
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: toluene / 17 h / 0 - 20 °C / Inert atmosphere
2.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.33 h / -78 °C / Inert atmosphere
2.2: 0.5 h / -78 - 20 °C / Inert atmosphere
3.1: (-)-diisopinocamphenylborane chloride / tetrahydrofuran / 2.33 h / -30 - 20 °C / Inert atmosphere
4.1: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere
5.1: camphor-10-sulfonic acid / dichloromethane; methanol / 0.5 h / 0 °C / Inert atmosphere
6.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 1 h / 0 - 20 °C / Inert atmosphere
7.1: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / water; ethanol / 2 h / 0 - 20 °C / Inert atmosphere
With
2,6-dimethylpyridine; oxalyl dichloride; hexaammonium heptamolybdate tetrahydrate; camphor-10-sulfonic acid; dihydrogen peroxide; dimethyl sulfoxide; triphenylphosphine; (-)-diisopinocamphenylborane chloride; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene;
6.1: |Mitsunobu Displacement;
DOI:10.1002/anie.201206560