C₄₈H₄₆F₂O₆

Base Information

Chemical Name:C₄₈H₄₆F₂O₆
CAS No.:1413373-52-0
Molecular Formula:C₄₈H₄₆F₂O₆
Molecular Weight:756.886
Hs Code.:

C<sub>48</sub>H<sub>46</sub>F<sub>2</sub>O<sub>6</sub>

Synonyms:C₄₈H₄₆F₂O₆

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Chemical Property of C₄₈H₄₆F₂O₆

Chemical Property:

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Technology Process of C₄₈H₄₆F₂O₆

There total 13 articles about C₄₈H₄₆F₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1413373-50-8
C₄₈H₄₆O₇

: 1413373-52-0
C₄₈H₄₆F₂O₆

Guidance literature:: With diethylamino-sulfur trifluoride; at 70 ℃; Inert atmosphere;

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 1413373-52-0
C₄₈H₄₆F₂O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: acetic anhydride; dimethyl sulfoxide / dimethyl sulfoxide / 20 °C / Inert atmosphere

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: -78 - 0 °C

2.3: cooling with ice

3.1: sodium tetrahydroborate / tetrahydrofuran / 20 °C

4.1: trifluoroacetic anhydride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C

4.2: -78 - 0 °C

5.1: potassium carbonate / 18-crown-6 ether / toluene / 20 °C

6.1: L-Selectride / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

6.2: 0.25 h

7.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 0.5 h / 0 °C / Inert atmosphere

8.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

8.2: 3 h / 0 - 20 °C

9.1: Dess-Martin periodane / 20 °C

10.1: diethylamino-sulfur trifluoride / 70 °C / Inert atmosphere

With sodium tetrahydroborate; n-butyllithium; tributylphosphine; diethylamino-sulfur trifluoride; dimethylsulfide borane complex; acetic anhydride; L-Selectride; potassium carbonate; Dess-Martin periodane; dimethyl sulfoxide; trifluoroacetic anhydride; 1,1'-azodicarbonyl-dipiperidine; 18-crown-6 ether; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; toluene; 7.1: Mitsunobu reaction;

Reference yield:

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 1413373-52-0
C₄₈H₄₆F₂O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 - 0 °C

1.3: cooling with ice

2.1: sodium tetrahydroborate / tetrahydrofuran / 20 °C

3.1: trifluoroacetic anhydride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C

3.2: -78 - 0 °C

4.1: potassium carbonate / 18-crown-6 ether / toluene / 20 °C

5.1: L-Selectride / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

5.2: 0.25 h

6.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 0.5 h / 0 °C / Inert atmosphere

7.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.2: 3 h / 0 - 20 °C

8.1: Dess-Martin periodane / 20 °C

9.1: diethylamino-sulfur trifluoride / 70 °C / Inert atmosphere

With sodium tetrahydroborate; n-butyllithium; tributylphosphine; diethylamino-sulfur trifluoride; dimethylsulfide borane complex; L-Selectride; potassium carbonate; Dess-Martin periodane; dimethyl sulfoxide; trifluoroacetic anhydride; 1,1'-azodicarbonyl-dipiperidine; 18-crown-6 ether; In tetrahydrofuran; hexane; dichloromethane; toluene; 6.1: Mitsunobu reaction;