N-(5-(1-cyano-2-(phenylamino)-2-thioxoethyl)-1,3,4-thiadiazol-2-yl)dodecanamide

Base Information

Chemical Name:N-(5-(1-cyano-2-(phenylamino)-2-thioxoethyl)-1,3,4-thiadiazol-2-yl)dodecanamide
CAS No.:1584679-89-9
Molecular Formula:C₂₃H₃₁N₅OS₂
Molecular Weight:457.664
Hs Code.:

Synonyms:N-(5-(1-cyano-2-(phenylamino)-2-thioxoethyl)-1,3,4-thiadiazol-2-yl)dodecanamide

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Chemical Property of N-(5-(1-cyano-2-(phenylamino)-2-thioxoethyl)-1,3,4-thiadiazol-2-yl)dodecanamide

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Technology Process of N-(5-(1-cyano-2-(phenylamino)-2-thioxoethyl)-1,3,4-thiadiazol-2-yl)dodecanamide

There total 3 articles about N-(5-(1-cyano-2-(phenylamino)-2-thioxoethyl)-1,3,4-thiadiazol-2-yl)dodecanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1584679-81-1
N-[5-(cyanomethyl)-1,3,4-thiadiazol-2-yl]dodecanamide

: 103-72-0
phenyl isothiocyanate

: 1584679-89-9
N-(5-(1-cyano-2-(phenylamino)-2-thioxoethyl)-1,3,4-thiadiazol-2-yl)dodecanamide

Guidance literature:: N-[5-(cyanomethyl)-1,3,4-thiadiazol-2-yl]dodecanamide; With potassium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

phenyl isothiocyanate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1080/00397911.2013.846381

Reference yield:

: 112-16-3
n-dodecanoyl chloride

: 1584679-89-9
N-(5-(1-cyano-2-(phenylamino)-2-thioxoethyl)-1,3,4-thiadiazol-2-yl)dodecanamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,4-dioxane / 0.5 h / Reflux

2.1: 2 h / Reflux

3.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.2: 12 h / 20 °C

With potassium hydroxide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1080/00397911.2013.846381

Reference yield:

: 1584679-80-0
1-(2-cyanoacetyl)-4-dodecanoyl thiosemicarbazide

: 1584679-89-9
N-(5-(1-cyano-2-(phenylamino)-2-thioxoethyl)-1,3,4-thiadiazol-2-yl)dodecanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / 1.17 h / 0 °C

2.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 12 h / 20 °C

With sulfuric acid; potassium hydroxide; In N,N-dimethyl-formamide;
DOI:10.1080/00397911.2013.846381