Technology Process of C40H58O8SSi
There total 12 articles about C40H58O8SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2,2-dimethyl-1-phenylsulphonyl-butan-3-one;
With
lithium diisopropyl amide;
In
tetrahydrofuran;
at -78 ℃;
for 1.5h;
C28H42O5Si;
In
tetrahydrofuran;
at -78 ℃;
for 0.25h;
DOI:10.1055/s-0030-1260784
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water / 2 h / 20 °C
2.1: lithium diisopropyl amide / tetrahydrofuran / 1.5 h / -78 °C
2.2: 0.25 h / -78 °C
With
sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide; lithium diisopropyl amide;
In
tetrahydrofuran; water;
2.2: Aldol condensation;
DOI:10.1055/s-0030-1260784
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water / 2 h / 20 °C
2.1: boron trifluoride diethyl etherate / toluene / 0.5 h / -78 °C
3.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C
4.1: sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water / 2 h / 20 °C
5.1: lithium diisopropyl amide / tetrahydrofuran / 1.5 h / -78 °C
5.2: 0.25 h / -78 °C
With
1H-imidazole; sodium periodate; osmium(VIII) oxide; boron trifluoride diethyl etherate; 4-methylmorpholine N-oxide; lithium diisopropyl amide;
In
tetrahydrofuran; water; N,N-dimethyl-formamide; toluene;
5.2: Aldol condensation;
DOI:10.1055/s-0030-1260784
