(+)-(5S,6S)-6-Hydroxy-5-trimethylsilyloxy-5,6-dihydro-β-ionylidenaethanol

Base Information

Chemical Name:(+)-(5S,6S)-6-Hydroxy-5-trimethylsilyloxy-5,6-dihydro-β-ionylidenaethanol
CAS No.:81757-21-3
Molecular Formula:C₁₈H₃₄O₃Si
Molecular Weight:326.552
Hs Code.:

Synonyms:(+)-(5S,6S)-6-Hydroxy-5-trimethylsilyloxy-5,6-dihydro-β-ionylidenaethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(5S,6S)-6-Hydroxy-5-trimethylsilyloxy-5,6-dihydro-β-ionylidenaethanol

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Technology Process of (+)-(5S,6S)-6-Hydroxy-5-trimethylsilyloxy-5,6-dihydro-β-ionylidenaethanol

There total 1 articles about (+)-(5S,6S)-6-Hydroxy-5-trimethylsilyloxy-5,6-dihydro-β-ionylidenaethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2E,4E)-5-((1S,6S)-1-Hydroxy-2,2,6-trimethyl-6-trimethylsilanyloxy-cyclohexyl)-3-methyl-penta-2,4-dienoic acid methyl ester

: (+)-(1'S,6'S,2Z,4E)-3-Methyl-5-<1'-hydroxy-2',2',6'-trimethyl-6'-trimethylsilyloxy-1'-cyclohexyl>-2,4-pentadienol

: 81757-21-3
(+)-(5S,6S)-6-Hydroxy-5-trimethylsilyloxy-5,6-dihydro-β-ionylidenaethanol

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; for 1.5h; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1002/hlca.19820650137

Reference yield: 74.0%

: 81757-21-3
(+)-(5S,6S)-6-Hydroxy-5-trimethylsilyloxy-5,6-dihydro-β-ionylidenaethanol

: 81757-22-4
(+)-(5S,6S)-6-Hydroxy-5-trimethylsilyloxy-5,6-dihydro-β-ionylidenaethanal

Guidance literature:: With manganese(IV) oxide; In ethyl acetate; for 0.5h; Ambient temperature;
DOI:10.1002/hlca.19820650137

Reference yield:

: 81757-21-3
(+)-(5S,6S)-6-Hydroxy-5-trimethylsilyloxy-5,6-dihydro-β-ionylidenaethanol

: (+)-(5S,6S)-6-Hydroxy-5-trimethylsilyloxy-5,6-dihydrovitamin-A-saeure-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / MnO₂ / ethyl acetate / 0.5 h / Ambient temperature

2: 80 percent / KOH / tetrahydrofuran / 2.5 h / Ambient temperature

With manganese(IV) oxide; potassium hydroxide; In tetrahydrofuran; ethyl acetate;
DOI:10.1002/hlca.19820650137