C₂₆H₄₀OSi

Base Information

Chemical Name:C₂₆H₄₀OSi
CAS No.:934808-34-1
Molecular Formula:C₂₆H₄₀OSi
Molecular Weight:396.689
Hs Code.:

Synonyms:C₂₆H₄₀OSi

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Chemical Property of C₂₆H₄₀OSi

Chemical Property:

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Technology Process of C₂₆H₄₀OSi

There total 3 articles about C₂₆H₄₀OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 934808-33-0
C₂₆H₃₈OSi

: 934808-34-1
C₂₆H₄₀OSi

Guidance literature:: With palladium on activated charcoal; hydrogen; In tetrahydrofuran; methanol; at 25 ℃; for 7h;
DOI:10.1021/ol070298z

Reference yield:

: C₂₃H₃₂O₂Si

: 934808-34-1
C₂₆H₄₀OSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: 93 percent / H₂ / irridium catalyst / CH₂Cl₂ / 4 h / 25 °C / 38002.6 Torr

2.1: oxalyl chloride; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

2.2: 83 percent / KHMDS / tetrahydrofuran; toluene / 1 h / -78 °C

3.1: 99 percent / H₂; Pd/C / methanol; tetrahydrofuran / 7 h / 25 °C

With palladium on activated charcoal; oxalyl dichloride; hydrogen; dimethyl sulfoxide; triethylamine; irridium catalyst; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol070298z

Reference yield:

: 157837-64-4
(2R,4S)-5-{[tert-butyl(diphenyl)silyl]oxy}-2,4-dimethylpentan-1-ol

: 934808-34-1
C₂₆H₄₀OSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl chloride; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

1.2: 83 percent / KHMDS / tetrahydrofuran; toluene / 1 h / -78 °C

2.1: 99 percent / H₂; Pd/C / methanol; tetrahydrofuran / 7 h / 25 °C

With palladium on activated charcoal; oxalyl dichloride; hydrogen; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol070298z