Methyl-2paraanisyl-2penten-3al

Base Information

Chemical Name:Methyl-2paraanisyl-2penten-3al
CAS No.:42762-66-3
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:

Synonyms:Methyl-2paraanisyl-2penten-3al

Suppliers and Price of Methyl-2paraanisyl-2penten-3al

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Methyl-2paraanisyl-2penten-3al

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Methyl-2paraanisyl-2penten-3al

There total 3 articles about Methyl-2paraanisyl-2penten-3al which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1319687-40-5
2-(4-methoxyphenyl)-2-methylpent-4-enal

: 42762-66-3
Methyl-2paraanisyl-2penten-3al

Guidance literature:: With hydrogen; In acetone; at 60 ℃; for 17h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1002/anie.201500596

Reference yield:

: C₁₄H₁₈O₃

: 42762-66-3
Methyl-2paraanisyl-2penten-3al

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 - 20 °C / Inert atmosphere

2.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

2.2: 0.33 h / 20 °C / Inert atmosphere

3.1: hydrogen / acetone / 17 h / 60 °C / Inert atmosphere; Schlenk technique; Sealed tube

With lithium aluminium tetrahydride; oxalyl dichloride; hydrogen; dimethyl sulfoxide; In diethyl ether; dichloromethane; acetone;
DOI:10.1002/anie.201500596

Reference yield:

: C₁₃H₁₈O₂

: 42762-66-3
Methyl-2paraanisyl-2penten-3al

Guidance literature:: Multi-step reaction with 2 steps

1.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

1.2: 0.33 h / 20 °C / Inert atmosphere

2.1: hydrogen / acetone / 17 h / 60 °C / Inert atmosphere; Schlenk technique; Sealed tube

With oxalyl dichloride; hydrogen; dimethyl sulfoxide; In dichloromethane; acetone;
DOI:10.1002/anie.201500596