(S)-1-(4-chlorobenzyl)-6-(3-mehyl-4-isopropoxyphenylimino)-3-(2-hydroxycarbonyl-2-hydro xyethyl)-1,3,5-triazinane-2,4-dion

Base Information

Chemical Name:(S)-1-(4-chlorobenzyl)-6-(3-mehyl-4-isopropoxyphenylimino)-3-(2-hydroxycarbonyl-2-hydro xyethyl)-1,3,5-triazinane-2,4-dion
CAS No.:1360117-48-1
Molecular Formula:C₂₃H₂₅ClN₄O₆
Molecular Weight:488.928
Hs Code.:

Synonyms:(S)-1-(4-chlorobenzyl)-6-(3-mehyl-4-isopropoxyphenylimino)-3-(2-hydroxycarbonyl-2-hydro xyethyl)-1,3,5-triazinane-2,4-dion

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Chemical Property of (S)-1-(4-chlorobenzyl)-6-(3-mehyl-4-isopropoxyphenylimino)-3-(2-hydroxycarbonyl-2-hydro xyethyl)-1,3,5-triazinane-2,4-dion

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Technology Process of (S)-1-(4-chlorobenzyl)-6-(3-mehyl-4-isopropoxyphenylimino)-3-(2-hydroxycarbonyl-2-hydro xyethyl)-1,3,5-triazinane-2,4-dion

There total 4 articles about (S)-1-(4-chlorobenzyl)-6-(3-mehyl-4-isopropoxyphenylimino)-3-(2-hydroxycarbonyl-2-hydro xyethyl)-1,3,5-triazinane-2,4-dion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1360116-54-6
(S)-1-(4-chlorobenzyl)-6-(3-mehyl-4-isopropoxyphenylimino)-3-(2-hydroxycarbonyl-2-methoxyethyl)-1,3,5-triazinane-2,4-dion

: 1360117-48-1
(S)-1-(4-chlorobenzyl)-6-(3-mehyl-4-isopropoxyphenylimino)-3-(2-hydroxycarbonyl-2-hydro xyethyl)-1,3,5-triazinane-2,4-dion

Guidance literature:: With chloro-trimethyl-silane; sodium iodide; In acetonitrile; for 4h; Reflux;

Reference yield:

: 1094544-66-7
3-methyl-4-isopropoxyaniline

: 1360117-48-1
(S)-1-(4-chlorobenzyl)-6-(3-mehyl-4-isopropoxyphenylimino)-3-(2-hydroxycarbonyl-2-hydro xyethyl)-1,3,5-triazinane-2,4-dion

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / tert-butyl alcohol / 8 h / Reflux

2: lithium hydroxide / methanol; tetrahydrofuran / 0.5 h / 60 °C

3: chloro-trimethyl-silane; sodium iodide / acetonitrile / 4 h / Reflux

With chloro-trimethyl-silane; acetic acid; sodium iodide; lithium hydroxide; In tetrahydrofuran; methanol; acetonitrile; tert-butyl alcohol;

Reference yield:

: 1360106-11-1
(S)-1-(4-chlorobenzyl)-6-(ethylthio)-3-(2-methoxycarbonyl-2-methoxy-ethyl)-1,3,5-triazine-2,4(1H,3H)-dion

: 1360117-48-1
(S)-1-(4-chlorobenzyl)-6-(3-mehyl-4-isopropoxyphenylimino)-3-(2-hydroxycarbonyl-2-hydro xyethyl)-1,3,5-triazinane-2,4-dion

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / tert-butyl alcohol / 8 h / Reflux

2: lithium hydroxide / methanol; tetrahydrofuran / 0.5 h / 60 °C

3: chloro-trimethyl-silane; sodium iodide / acetonitrile / 4 h / Reflux

With chloro-trimethyl-silane; acetic acid; sodium iodide; lithium hydroxide; In tetrahydrofuran; methanol; acetonitrile; tert-butyl alcohol;