C₁₅H₂₂N₈O₇

Base Information

• Chemical Name: C₁₅H₂₂N₈O₇
• CAS No.: 128424-99-7
• Molecular Formula: C₁₅H₂₂N₈O₇
• Molecular Weight: 426.389
• Mol file: 128424-99-7.mol

Synonyms:C₁₅H₂₂N₈O₇

Chemical Property of C₁₅H₂₂N₈O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₂₂N₈O₇

There total 31 articles about C₁₅H₂₂N₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-arginine (74-79-3,25212-18-4) + N-(2,4-dinitro-5-fluorophenyl)-L-alaninamide (95713-52-3) → C15H22N8O7 (128424-99-7)

Guidance literature:

With sodium hydrogencarbonate; In water; acetone;

DOI:10.1021/np900340t

Reference yield:

micropeptin LH911A + N-(2,4-dinitro-5-fluorophenyl)-L-alaninamide (95713-52-3) → (2S,3S)-2-(5-((S)-1-amino-1-oxopropan-2-ylamino)-2,4-dinitrophenylamino)-3-methylpentanoic acid + L-FDAA-L-Thr + C15H22N8O7 (128424-99-7) + L-FDAA-N-methyl-Phe (194736-58-8) + (S)-2-(5-((S)-1-amino-1-oxopropan-2-ylamino)-2,4-dinitrophenylamino)-3-methylbutanoic acid

Guidance literature:

micropeptin LH₉₁₁A; With hydrogenchloride; water; at 110 ℃; for 16h; Sealed tube;

N-(2,4-dinitro-5-fluorophenyl)-L-alaninamide; With sodium hydrogencarbonate; In water; acetone; at 70 ℃; for 2h;

DOI:10.1016/j.tet.2013.09.054

Reference yield:

micropeptin LH911B + N-(2,4-dinitro-5-fluorophenyl)-L-alaninamide (95713-52-3) → (2S,3S)-2-(5-((S)-1-amino-1-oxopropan-2-ylamino)-2,4-dinitrophenylamino)-3-methylpentanoic acid + L-FDAA-L-Thr + C15H22N8O7 (128424-99-7) + L-FDAA-N-methyl-Phe (194736-58-8) + (S)-2-(5-((S)-1-amino-1-oxopropan-2-ylamino)-2,4-dinitrophenylamino)-3-methylbutanoic acid

Guidance literature:

micropeptin LH₉₁₁B; With hydrogenchloride; water; at 110 ℃; for 16h; Sealed tube;

N-(2,4-dinitro-5-fluorophenyl)-L-alaninamide; With sodium hydrogencarbonate; In water; acetone; at 70 ℃; for 2h;

DOI:10.1016/j.tet.2013.09.054

upstream raw materials:

L-arginine

N-(2,4-dinitro-5-fluorophenyl)-L-alaninamide

micropeptin MZ₈₄₅

micropeptin MZ₈₅₉

Refernces

• 1、 Matsuo, Yoshihide,Kanoh, Kaneo,Jang, Jae-Hyuk,Adachi, Kyoko,Matsuda, Satoru,Miki, Osamu,Kato, Toshiaki,Shizuri, Yoshikazu. "Streptobactin, a tricatechol-type siderophore from marine-derived streptomyces sp. YM5-799". . p. 2371 - 2376. Retrieved 2011.
• 2、 Sanz, Miriam,Salinas, Roberto Kopke,Pinto, Ernani. "Namalides B and C and Spumigins K-N from the Cultured Freshwater Cyanobacterium Sphaerospermopsis torques-reginae". . p. 2492 - 2501. Retrieved 2017/09/27.
• 3、 Vegman, Margarita,Carmeli, Shmuel. "Eight micropeptins from a Microcystis spp. bloom collected from a fishpond near Kibbutz Lehavot HaBashan, Israel". . p. 10108 - 10115. Retrieved 2013/11/06.