F₂B(CH₃CH₂(H₃C)2C₄NC(C₆H₄I)C₄N(CH₃)(CH₂CH₃)CH₂C₂HN₃CONHCH₂CH(SO₃H)CONHCH₂COOH)

Base Information

• Chemical Name: F₂B(CH₃CH₂(H₃C)2C₄NC(C₆H₄I)C₄N(CH₃)(CH₂CH₃)CH₂C₂HN₃CONHCH₂CH(SO₃H)CONHCH₂COOH)
• CAS No.: 1379516-54-7
• Molecular Formula: C₃₁H₃₅BF₂IN₇O₇S
• Molecular Weight: 825.44
• Mol file: 1379516-54-7.mol

Synonyms:F₂B(CH₃CH₂(H₃C)2C₄NC(C₆H₄I)C₄N(CH₃)(CH₂CH₃)CH₂C₂HN₃CONHCH₂CH(SO₃H)CONHCH₂COOH)

Chemical Property of F₂B(CH₃CH₂(H₃C)2C₄NC(C₆H₄I)C₄N(CH₃)(CH₂CH₃)CH₂C₂HN₃CONHCH₂CH(SO₃H)CONHCH₂COOH)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of F₂B(CH₃CH₂(H₃C)2C₄NC(C₆H₄I)C₄N(CH₃)(CH₂CH₃)CH₂C₂HN₃CONHCH₂CH(SO₃H)CONHCH₂COOH)

There total 3 articles about F₂B(CH₃CH₂(H₃C)2C₄NC(C₆H₄I)C₄N(CH₃)(CH₂CH₃)CH₂C₂HN₃CONHCH₂CH(SO₃H)CONHCH₂COOH) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

C23H25BF2IN5 + HCCCONHCH2CH(SO3H)CONHCH2COOH (1379514-83-6) → F2B(CH3CH2(H3C)2C4NC(C6H4I)C4N(CH3)(CH2CH3)CH2C2HN3CONHCH2CH(SO3H)CONHCH2COOH) (1379516-54-7)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; dimethyl sulfoxide; at 20 ℃;

DOI:10.1039/c2ob25428j

Reference yield:

C23H25BBrF2IN2 → F2B(CH3CH2(H3C)2C4NC(C6H4I)C4N(CH3)(CH2CH3)CH2C2HN3CONHCH2CH(SO3H)CONHCH2COOH) (1379516-54-7)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium azide / dichloromethane; N,N-dimethyl-formamide / 1 h

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; dimethyl sulfoxide / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 2: Huisgen 1,3-dipolar cycloaddition;

DOI:10.1039/c2ob25428j

Reference yield:

2,6-diethyl-4,4-difluoro-1,3,5,7-tetramethyl-8-(4-iodophenyl)-4-bora-3a,4a-diaza-s-indacene → F2B(CH3CH2(H3C)2C4NC(C6H4I)C4N(CH3)(CH2CH3)CH2C2HN3CONHCH2CH(SO3H)CONHCH2COOH) (1379516-54-7)

Guidance literature:

Multi-step reaction with 3 steps

1: N-Bromosuccinimide / dichloromethane / 0.5 h / 20 °C

2: sodium azide / dichloromethane; N,N-dimethyl-formamide / 1 h

3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; dimethyl sulfoxide / 20 °C

With N-Bromosuccinimide; sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 3: Huisgen 1,3-dipolar cycloaddition;

DOI:10.1039/c2ob25428j

upstream raw materials:

HCCCONHCH₂CH(SO₃H)CONHCH₂COOH