ethyl 6-bromo-2-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]-5-methoxy-1-benzofuran-3-carboxylate

Base Information

Chemical Name:ethyl 6-bromo-2-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]-5-methoxy-1-benzofuran-3-carboxylate
CAS No.:123647-74-5
Molecular Formula:C₂₁H₁₆BrNO₆
Molecular Weight:458.265
Hs Code.:
Mol file:123647-74-5.mol

Synonyms:2-phthalimidomethyl-3-ethoxycarbonyl-5-methoxy-6-bromobenzofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 6-bromo-2-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]-5-methoxy-1-benzofuran-3-carboxylate

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Technology Process of ethyl 6-bromo-2-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]-5-methoxy-1-benzofuran-3-carboxylate

There total 1 articles about ethyl 6-bromo-2-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]-5-methoxy-1-benzofuran-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.3%

: 85388-65-4
2-bromomethyl-3-ethoxycarbonyl-5-methoxy-6-bromobenzofuran

: 1074-82-4
potassium phtalimide

: 123647-74-5
2-phthalimidomethyl-3-ethoxycarbonyl-5-methoxy-6-bromobenzofuran

Guidance literature:: In N,N-dimethyl-formamide; at 50 - 60 ℃; for 6h;
DOI:10.1007/BF00764468

Reference yield:

: 123647-74-5
2-phthalimidomethyl-3-ethoxycarbonyl-5-methoxy-6-bromobenzofuran

: 1445-69-8
1,4-dihydroxyphthalazine

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH, ethanol / 2 h / Heating

2: hydrazine hydrate / ethanol / 7 h / Heating

With sodium hydroxide; ethanol; hydrazine hydrate; In ethanol;
DOI:10.1007/BF00764468