Technology Process of C13H18O3
There total 5 articles about C13H18O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 23 ℃;
for 2h;
Inert atmosphere;
DOI:10.1002/ejoc.201001281
- Guidance literature:
-
Multi-step reaction with 4 steps
1: palladium 10% on activated carbon; hydrogen / methanol / 0.5 h / 23 °C
2: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere
3: tetrahydrofuran / 2 h / -78 - 23 °C / Inert atmosphere
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 23 °C / Inert atmosphere
With
palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; diisobutylaluminium hydride;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1002/ejoc.201001281
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere
2: tetrahydrofuran / 2 h / -78 - 23 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 23 °C / Inert atmosphere
With
tetrabutyl ammonium fluoride; diisobutylaluminium hydride;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1002/ejoc.201001281
