N-ethyl-N-(9-o-tolyl-6-(2-(trimethylsilyl)ethynyl)-3H-xanthen-3-ylidene)ethanaminium chloride

Base Information

• Chemical Name: N-ethyl-N-(9-o-tolyl-6-(2-(trimethylsilyl)ethynyl)-3H-xanthen-3-ylidene)ethanaminium chloride
• CAS No.: 1169852-10-1
• Molecular Formula: C₂₉H₃₂NOSi*Cl
• Molecular Weight: 474.118
• Mol file: 1169852-10-1.mol

Synonyms:N-ethyl-N-(9-o-tolyl-6-(2-(trimethylsilyl)ethynyl)-3H-xanthen-3-ylidene)ethanaminium chloride

Chemical Property of N-ethyl-N-(9-o-tolyl-6-(2-(trimethylsilyl)ethynyl)-3H-xanthen-3-ylidene)ethanaminium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-ethyl-N-(9-o-tolyl-6-(2-(trimethylsilyl)ethynyl)-3H-xanthen-3-ylidene)ethanaminium chloride

There total 1 articles about N-ethyl-N-(9-o-tolyl-6-(2-(trimethylsilyl)ethynyl)-3H-xanthen-3-ylidene)ethanaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ortho-tolylmagnesium bromide (932-31-0) + 3-(diethylamino)-6-(2-(trimethylsilyl)ethynyl)-9H-xanthen-9-one (1169852-00-9) → N-ethyl-N-(9-o-tolyl-6-(2-(trimethylsilyl)ethynyl)-3H-xanthen-3-ylidene)ethanaminium chloride (1169852-10-1)

Guidance literature:

ortho-tolylmagnesium bromide; 3-(diethylamino)-6-(2-(trimethylsilyl)ethynyl)-9H-xanthen-9-one; In tetrahydrofuran; diethyl ether; at 50 ℃; for 12h; Inert atmosphere;

With hydrogenchloride; In dichloromethane; water; for 0.0833333h;

DOI:10.1021/ol9010344

Reference yield:

N-ethyl-N-(9-o-tolyl-6-(2-(trimethylsilyl)ethynyl)-3H-xanthen-3-ylidene)ethanaminium chloride (1169852-10-1) → C26H24NO(1+)*Cl(1-) (1169852-07-6)

Guidance literature:

With sodium hydroxide; In methanol; water; at 20 ℃; for 1h;

DOI:10.1021/ol9010344

upstream raw materials:

ortho-tolylmagnesium bromide

3-(diethylamino)-6-(2-(trimethylsilyl)ethynyl)-9H-xanthen-9-one

Downstream raw materials:

C₂₆H₂₄NO⁽¹⁺⁾*Cl^(1-)