4-(N,N-dimethylamino)-N-(3-methyl-4-phenylthiazolio-2-methylidene) aniline iodide

Base Information

• Chemical Name: 4-(N,N-dimethylamino)-N-(3-methyl-4-phenylthiazolio-2-methylidene) aniline iodide
• CAS No.: 5960-22-5
• Molecular Formula: C₁₉H₂₀N₃S*I
• Molecular Weight: 449.358

Synonyms:4-(N,N-dimethylamino)-N-(3-methyl-4-phenylthiazolio-2-methylidene) aniline iodide

Chemical Property of 4-(N,N-dimethylamino)-N-(3-methyl-4-phenylthiazolio-2-methylidene) aniline iodide

Chemical Property:

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Technology Process of 4-(N,N-dimethylamino)-N-(3-methyl-4-phenylthiazolio-2-methylidene) aniline iodide

There total 2 articles about 4-(N,N-dimethylamino)-N-(3-methyl-4-phenylthiazolio-2-methylidene) aniline iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dimethyl-4-phenylthiazolium iodide (5968-24-1) + p-dimethylaminonitrosobenzene (138-89-6) → 4-(N,N-dimethylamino)-N-(3-methyl-4-phenylthiazolio-2-methylidene) aniline iodide (5960-22-5)

Guidance literature:

With piperidine; In methanol; at 30 ℃; Kinetics; Thermodynamic data; Mechanism; further temperatures; E_a;

Reference yield:

2,3-dimethyl-4-nitroso-aniline (871876-73-2) + 2,3-dimethyl-4-phenylthiazolium iodide (5968-24-1) → 4-(N,N-dimethylamino)-N-(3-methyl-4-phenylthiazolio-2-methylidene) aniline iodide (5960-22-5)

Guidance literature:

With piperidine; ethanol;

Reference yield:

4-(N,N-dimethylamino)-N-(3-methyl-4-phenylthiazolio-2-methylidene) aniline iodide (5960-22-5) → 4-amino-N,N-dimethylaniline (99-98-9) + 2-Formyl-3-methyl-4-phenyl-thiazol-3-ium; iodide

Guidance literature:

With sodium hydroxide; In methanol; at 10 - 25 ℃; Kinetics; Thermodynamic data; E_a;

DOI:10.1007/BF00646717

upstream raw materials:

2,3-dimethyl-4-nitroso-aniline

2,3-dimethyl-4-phenylthiazolium iodide

p-dimethylaminonitrosobenzene

Downstream raw materials:

1,3-bis-(3-methyl-4-phenyl-thiazol-2-yl)-1,2-diaza-trimethinium; iodide

3-methyl-2-{[(3-methyl-3H-benzothiazol-2-ylidene)-hydrazono]-methyl}-4-phenyl-thiazolium; iodide

3-methyl-2-{[(3-methyl-4,5-diphenyl-3H-thiazol-2-ylidene)-hydrazono]-methyl}-4-phenyl-thiazolium; iodide

4-amino-N,N-dimethylaniline

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