2-(1-Hydroxy-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethyl)-2-phenyl-malonic acid diethyl ester; hydrochloride

Base Information

Chemical Name:2-(1-Hydroxy-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethyl)-2-phenyl-malonic acid diethyl ester; hydrochloride
CAS No.:105843-24-1
Molecular Formula:C₂₂H₃₁NO₅*ClH
Molecular Weight:425.953
Hs Code.:

Synonyms:2-(1-Hydroxy-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethyl)-2-phenyl-malonic acid diethyl ester; hydrochloride

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Chemical Property of 2-(1-Hydroxy-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethyl)-2-phenyl-malonic acid diethyl ester; hydrochloride

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Technology Process of 2-(1-Hydroxy-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethyl)-2-phenyl-malonic acid diethyl ester; hydrochloride

There total 3 articles about 2-(1-Hydroxy-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethyl)-2-phenyl-malonic acid diethyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 105843-26-3
C₂₂H₃₀NO₅

: 105843-24-1
2-(1-Hydroxy-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethyl)-2-phenyl-malonic acid diethyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol;

Reference yield:

: 76893-32-8
3-(bromomethyl)-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-oxyl

: 105843-24-1
2-(1-Hydroxy-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethyl)-2-phenyl-malonic acid diethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / 2N NaOH / TBAH / CH₂Cl₂ / 16 h / Ambient temperature

2: 94 percent / HCl / ethanol

With hydrogenchloride; sodium hydroxide; tetra(n-butyl)ammonium hydroxide; In ethanol; dichloromethane;

Reference yield:

: 83-13-6
diethyl 2-phenylmalonate

: 105843-24-1
2-(1-Hydroxy-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethyl)-2-phenyl-malonic acid diethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / 2N NaOH / TBAH / CH₂Cl₂ / 16 h / Ambient temperature

2: 94 percent / HCl / ethanol

With hydrogenchloride; sodium hydroxide; tetra(n-butyl)ammonium hydroxide; In ethanol; dichloromethane;