C₇₀H₆₅N₇O₇S₃

Base Information

Chemical Name:C₇₀H₆₅N₇O₇S₃
CAS No.:1621326-21-3
Molecular Formula:C₇₀H₆₅N₇O₇S₃
Molecular Weight:1212.53
Hs Code.:

C<sub>70</sub>H<sub>65</sub>N<sub>7</sub>O<sub>7</sub>S<sub>3</sub>

Synonyms:C₇₀H₆₅N₇O₇S₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₇₀H₆₅N₇O₇S₃

Chemical Property:

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Technology Process of C₇₀H₆₅N₇O₇S₃

There total 10 articles about C₇₀H₆₅N₇O₇S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 68858-20-8
Fmoc-Val-OH

: 1621326-20-2
C₅₀H₄₆N₆O₄S₃

: 1621326-21-3
C₇₀H₆₅N₇O₇S₃

Guidance literature:: Fmoc-Val-OH; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; at 0 ℃; for 1h;

C₅₀H₄₆N₆O₄S₃; With dmap; In tetrahydrofuran; at 0 - 25 ℃; for 2h;

Reference yield:

: C₂₇H₂₂Cl₃NO₅

: 1621326-20-2
C₅₀H₄₆N₆O₄S₃

: 1621326-21-3
C₇₀H₆₅N₇O₇S₃

Guidance literature:: With dmap; In tetrahydrofuran; at 0 - 25 ℃; for 2h;
DOI:10.1016/j.bmcl.2014.07.006

Reference yield:

: 1621325-96-9
C₂₈H₂₉N₃O₄S₂

: 1621326-21-3
C₇₀H₆₅N₇O₇S₃

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 25 °C

2: dmap; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / acetonitrile / 4 h / 25 °C

3: dmap / tetrahydrofuran / 2 h / 0 - 25 °C

With dmap; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2014.07.006