3-(3-phthalimido)propyl-4'-(1-methoxy-cyclohexyloxy)-5'-(1-methoxy-cyclohexyloxymethyl)-thymidine

Base Information

• Chemical Name: 3-(3-phthalimido)propyl-4'-(1-methoxy-cyclohexyloxy)-5'-(1-methoxy-cyclohexyloxymethyl)-thymidine
• CAS No.: 1021905-33-8
• Molecular Formula: C₃₅H₄₇N₃O₉
• Molecular Weight: 653.773

Synonyms:3-(3-phthalimido)propyl-4'-(1-methoxy-cyclohexyloxy)-5'-(1-methoxy-cyclohexyloxymethyl)-thymidine

Chemical Property of 3-(3-phthalimido)propyl-4'-(1-methoxy-cyclohexyloxy)-5'-(1-methoxy-cyclohexyloxymethyl)-thymidine

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Technology Process of 3-(3-phthalimido)propyl-4'-(1-methoxy-cyclohexyloxy)-5'-(1-methoxy-cyclohexyloxymethyl)-thymidine

There total 1 articles about 3-(3-phthalimido)propyl-4'-(1-methoxy-cyclohexyloxy)-5'-(1-methoxy-cyclohexyloxymethyl)-thymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-(3-bromopropyl)isoindole-1,3-dione (5460-29-7) + 4-(1-methoxy-cyclohexyloxy)-5-(1-methoxy-cyclohexyloxymethyl)-thymidine (1021905-20-3) → 3-(3-phthalimido)propyl-4'-(1-methoxy-cyclohexyloxy)-5'-(1-methoxy-cyclohexyloxymethyl)-thymidine (1021905-33-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; acetone; at 20 - 50 ℃; for 102h;

DOI:10.1016/j.jfluchem.2009.07.003

Reference yield: 100.0%

3-(3-phthalimido)propyl-4'-(1-methoxy-cyclohexyloxy)-5'-(1-methoxy-cyclohexyloxymethyl)-thymidine (1021905-33-8) → 3-(3-Amino-propyl)-1-[(2R,4S,5R)-4-(1-methoxy-cyclohexyloxy)-5-(1-methoxy-cyclohexyloxymethyl)-tetrahydro-furan-2-yl]-5-methyl-1H-pyrimidine-2,4-dione (1021905-52-1)

Guidance literature:

With hydrazine; In ethanol; at 20 ℃; for 96h;

upstream raw materials:

2-(3-bromopropyl)isoindole-1,3-dione

4-(1-methoxy-cyclohexyloxy)-5-(1-methoxy-cyclohexyloxymethyl)-thymidine

Downstream raw materials:

3-(3-Amino-propyl)-1-[(2R,4S,5R)-4-(1-methoxy-cyclohexyloxy)-5-(1-methoxy-cyclohexyloxymethyl)-tetrahydro-furan-2-yl]-5-methyl-1H-pyrimidine-2,4-dione

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