4-[{4-butyl-6-(2-methoxyethoxy)-2-methylpyrimidin-5-yl}meth yl]-2,6-dipropyl phenol

Base Information

Chemical Name:4-[{4-butyl-6-(2-methoxyethoxy)-2-methylpyrimidin-5-yl}meth yl]-2,6-dipropyl phenol
CAS No.:1256780-49-0
Molecular Formula:C₂₅H₃₈N₂O₃
Molecular Weight:414.588
Hs Code.:

Synonyms:4-[{4-butyl-6-(2-methoxyethoxy)-2-methylpyrimidin-5-yl}meth yl]-2,6-dipropyl phenol

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Chemical Property of 4-[{4-butyl-6-(2-methoxyethoxy)-2-methylpyrimidin-5-yl}meth yl]-2,6-dipropyl phenol

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Technology Process of 4-[{4-butyl-6-(2-methoxyethoxy)-2-methylpyrimidin-5-yl}meth yl]-2,6-dipropyl phenol

There total 5 articles about 4-[{4-butyl-6-(2-methoxyethoxy)-2-methylpyrimidin-5-yl}meth yl]-2,6-dipropyl phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1256780-45-6
4-butyl-5-{4-(tert-butyldimethylsilyloxy)-3,5-dipropylbenzyl}-6-(2-methoxyethoxy)-2-methylpyrimidine

: 1256780-49-0
4-[{4-butyl-6-(2-methoxyethoxy)-2-methylpyrimidin-5-yl}meth yl]-2,6-dipropyl phenol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h; cooling with ice;

Reference yield:

: 137421-55-7
t-butyl-dimethylsilyloxy-2,6-dipropyl-4-hydroxymethyl benzene

: 1256780-49-0
4-[{4-butyl-6-(2-methoxyethoxy)-2-methylpyrimidin-5-yl}meth yl]-2,6-dipropyl phenol

Guidance literature:: Multi-step reaction with 5 steps

1.1: phosphorus tribromide / toluene / 1 h / 20 °C / cooling with ice

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

2.2: 18 h / 20 °C

3.1: sodium methylate / methanol / 6 h / Reflux

4.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 9 h / 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / cooling with ice

With tetrabutyl ammonium fluoride; sodium methylate; phosphorus tribromide; sodium hydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene; mineral oil; 4.1: Mitsunobu reaction;

Reference yield:

: 1256779-86-8
methyl 2-{4-(tert-butyldimethylsilyloxy)-3,5-dipropylbenzyl}-3-oxo heptanate

: 1256780-49-0
4-[{4-butyl-6-(2-methoxyethoxy)-2-methylpyrimidin-5-yl}meth yl]-2,6-dipropyl phenol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate / methanol / 6 h / Reflux

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 9 h / 20 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / cooling with ice

With tetrabutyl ammonium fluoride; sodium methylate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; 2: Mitsunobu reaction;