2,12-(boronic acid)-7-(4'-methoxyphenyl)-5,6,8,9-tetrahydrodibenz[c,h]acridine

Base Information

Chemical Name:2,12-(boronic acid)-7-(4'-methoxyphenyl)-5,6,8,9-tetrahydrodibenz[c,h]acridine
CAS No.:429696-57-1
Molecular Formula:C₂₈H₂₅B₂NO₅
Molecular Weight:477.132
Hs Code.:

Synonyms:2,12-(boronic acid)-7-(4'-methoxyphenyl)-5,6,8,9-tetrahydrodibenz[c,h]acridine

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Chemical Property of 2,12-(boronic acid)-7-(4'-methoxyphenyl)-5,6,8,9-tetrahydrodibenz[c,h]acridine

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Technology Process of 2,12-(boronic acid)-7-(4'-methoxyphenyl)-5,6,8,9-tetrahydrodibenz[c,h]acridine

There total 2 articles about 2,12-(boronic acid)-7-(4'-methoxyphenyl)-5,6,8,9-tetrahydrodibenz[c,h]acridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 429696-55-9
C₃₂H₃₃B₂NO₅

: 429696-57-1
2,12-(boronic acid)-7-(4'-methoxyphenyl)-5,6,8,9-tetrahydrodibenz[c,h]acridine

Guidance literature:: With potassium hydroxide; In ethanol; Heating;
DOI:10.1016/S0040-4020(01)01113-9

Reference yield:

: 2,12-dibromo-7-(4'-methoxyphenyl)-5,6,8,9-tetrahydrodibenzo[c,h]acridine

: 429696-57-1
2,12-(boronic acid)-7-(4'-methoxyphenyl)-5,6,8,9-tetrahydrodibenz[c,h]acridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -75 °C

1.2: 51 percent / tetrahydrofuran; hexane / -60 - 20 °C

2.1: 89 percent / KOH / ethanol / Heating

With potassium hydroxide; n-butyllithium; In tetrahydrofuran; ethanol; hexane;
DOI:10.1016/S0040-4020(01)01113-9

Reference yield:

: 51839-15-7
5-iodo-isophthalic acid dimethyl ester

: 429696-57-1
2,12-(boronic acid)-7-(4'-methoxyphenyl)-5,6,8,9-tetrahydrodibenz[c,h]acridine

: 175843-77-3
2,12-bis(3,5-bis(methoxycarbonyl)phenyl)-7-(4'-methoxyphenyl)-5,6,8,9-tetrahydrodibenz[c,h]acridine

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; for 24h; Heating;
DOI:10.1016/S0040-4020(01)01113-9