C₂₂H₂₀N₄O₆

Base Information

Chemical Name:C₂₂H₂₀N₄O₆
CAS No.:1109236-81-8
Molecular Formula:C₂₂H₂₀N₄O₆
Molecular Weight:436.424
Hs Code.:

C<sub>22</sub>H<sub>20</sub>N<sub>4</sub>O<sub>6</sub>

Synonyms:C₂₂H₂₀N₄O₆

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Chemical Property of C₂₂H₂₀N₄O₆

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Technology Process of C₂₂H₂₀N₄O₆

There total 7 articles about C₂₂H₂₀N₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1109237-15-1
C₄₁H₃₄N₄O₆

: 1109236-81-8
C₂₂H₂₀N₄O₆

Guidance literature:: C₄₁H₃₄N₄O₆; With trifluoroacetic acid; In dichloromethane;

With triethylsilane; In dichloromethane; for 0.666667h;
DOI:10.1016/j.bmc.2010.06.081

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1109236-81-8
C₂₂H₂₀N₄O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: tris-(o-tolyl)phosphine / palladium diacetate / N,N-dimethyl-formamide / 24 h / 130 °C / Inert atmosphere

2.1: sodium tetrahydroborate / ethanol / 20 °C

3.1: triethylamine / tetrahydrofuran / 1 h / 0 °C

4.1: sodium azide / N,N-dimethyl-formamide / 20 - 50 °C

4.2: 20 °C

5.1: hydrogenchloride / hexanes; diethyl ether / 20 °C

6.1: 4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 48 h / 20 °C

7.1: trifluoroacetic acid / dichloromethane / 20 °C

8.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 96 h / 20 °C

9.1: triethylsilane; trifluoroacetic acid / dichloromethane

With 4-methyl-morpholine; hydrogenchloride; triethylsilane; sodium tetrahydroborate; sodium azide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; tris-(o-tolyl)phosphine; trifluoroacetic acid; palladium diacetate; In tetrahydrofuran; hexanes; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: C₁₅H₂₀O₅S

: 1109236-81-8
C₂₂H₂₀N₄O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium azide / N,N-dimethyl-formamide / 20 - 50 °C

1.2: 20 °C

2.1: hydrogenchloride / hexanes; diethyl ether / 20 °C

3.1: 4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 48 h / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 20 °C

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 96 h / 20 °C

6.1: triethylsilane; trifluoroacetic acid / dichloromethane

With 4-methyl-morpholine; hydrogenchloride; triethylsilane; sodium azide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In hexanes; diethyl ether; dichloromethane; N,N-dimethyl-formamide;