5-(4-chlorophenyl)-3-isopropylimino-2-(3-pyridylamino)-3,5-dihydrophenazine

Base Information

Chemical Name:5-(4-chlorophenyl)-3-isopropylimino-2-(3-pyridylamino)-3,5-dihydrophenazine
CAS No.:1353730-91-2
Molecular Formula:C₂₆H₂₂ClN₅
Molecular Weight:439.947
Hs Code.:

Synonyms:5-(4-chlorophenyl)-3-isopropylimino-2-(3-pyridylamino)-3,5-dihydrophenazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(4-chlorophenyl)-3-isopropylimino-2-(3-pyridylamino)-3,5-dihydrophenazine

Chemical Property:

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Technology Process of 5-(4-chlorophenyl)-3-isopropylimino-2-(3-pyridylamino)-3,5-dihydrophenazine

There total 8 articles about 5-(4-chlorophenyl)-3-isopropylimino-2-(3-pyridylamino)-3,5-dihydrophenazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353740-44-9
5-(4-chlorophenyl)-3-imino-N-(pyridin-3-yl)-3,5-dihydrophenazin-2-amine

: 75-31-0
isopropylamine

: 1353730-91-2
5-(4-chlorophenyl)-3-isopropylimino-2-(3-pyridylamino)-3,5-dihydrophenazine

Guidance literature:: In 1,4-dioxane; at 110 ℃; for 7h; sealed bomb;

Reference yield:

: 106-47-8
4-chloro-aniline

: 1353730-91-2
5-(4-chlorophenyl)-3-isopropylimino-2-(3-pyridylamino)-3,5-dihydrophenazine

Guidance literature:: Multi-step reaction with 7 steps

1: potassium fluoride; potassium carbonate / 10 h / 160 °C

2: acetic acid; zinc / dichloromethane / 4 h / 20 °C

3: triethylamine / methanol / 5 h / Reflux

4: triethylamine / tetrahydrofuran / 28 h / Reflux; Inert atmosphere

5: acetic acid; zinc / methanol / 20 °C / Cooling with ice

6: acetic acid / methanol / 20 °C / Air

7: 1,4-dioxane / 7 h / 110 °C / Sealed tube

With potassium fluoride; potassium carbonate; acetic acid; triethylamine; zinc; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;
DOI:10.3390/molecules17044545

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1353730-91-2
5-(4-chlorophenyl)-3-isopropylimino-2-(3-pyridylamino)-3,5-dihydrophenazine

Guidance literature:: Multi-step reaction with 7 steps

1: potassium fluoride; potassium carbonate / 10 h / 160 °C

2: acetic acid; zinc / dichloromethane / 4 h / 20 °C

3: triethylamine / methanol / 5 h / Reflux

4: triethylamine / tetrahydrofuran / 28 h / Reflux; Inert atmosphere

5: acetic acid; zinc / methanol / 20 °C / Cooling with ice

6: acetic acid / methanol / 20 °C / Air

7: 1,4-dioxane / 7 h / 110 °C / Sealed tube

With potassium fluoride; potassium carbonate; acetic acid; triethylamine; zinc; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;
DOI:10.3390/molecules17044545