{4-[(4-Amino-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-carbamic acid tert-butyl ester

Base Information

Chemical Name:{4-[(4-Amino-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-carbamic acid tert-butyl ester
CAS No.:206656-46-4
Molecular Formula:C₄₂H₅₄N₄O₆Si
Molecular Weight:738.999
Hs Code.:

{4-[(4-Amino-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-carbamic acid tert-butyl ester

Synonyms:{4-[(4-Amino-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-carbamic acid tert-butyl ester

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Chemical Property of {4-[(4-Amino-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-carbamic acid tert-butyl ester

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Technology Process of {4-[(4-Amino-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-carbamic acid tert-butyl ester

There total 1 articles about {4-[(4-Amino-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 200395-40-0
(4-{[4-(Benzhydrylidene-amino)-phenyl]-tert-butoxycarbonyl-amino}-phenyl)-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-carbamic acid tert-butyl ester

: 206656-46-4
{4-[(4-Amino-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-carbamic acid tert-butyl ester

Guidance literature:: With ammonium formate; palladium on activated charcoal; In tetrahydrofuran; methanol; at 50 ℃; for 11h;
DOI:10.1021/ja980052c

Reference yield:

: 197144-27-7
4,4’-dibromo-N-(tert-butoxycarbonyl)phenylaniline

: 206656-46-4
{4-[(4-Amino-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-carbamic acid tert-butyl ester

: C₁₀₁H₁₂₃N₉O₁₄Si₂

Guidance literature:: With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); sodium t-butanolate; In toluene; at 80 ℃; for 27h;
DOI:10.1021/ja980052c

Reference yield:

: C₉₄H₁₀₈Br₂N₈O₁₆

: 206656-46-4
{4-[(4-Amino-phenyl)-tert-butoxycarbonyl-amino]-phenyl}-{4-[tert-butoxycarbonyl-(4-trimethylsilanyl-phenyl)-amino]-phenyl}-carbamic acid tert-butyl ester

: C₁₇₈H₂₁₄N₁₆O₂₈Si₂

Guidance literature:: With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); triethylamine; sodium t-butanolate; In toluene; at 90 ℃; for 18h;
DOI:10.1021/ja980052c