3-(4-bromophenyl)propanol sulfamate ester

Base Information

Chemical Name:3-(4-bromophenyl)propanol sulfamate ester
CAS No.:1072126-72-7
Molecular Formula:C₉H₁₂BrNO₃S
Molecular Weight:294.169
Hs Code.:

Synonyms:3-(4-bromophenyl)propanol sulfamate ester

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Chemical Property of 3-(4-bromophenyl)propanol sulfamate ester

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Technology Process of 3-(4-bromophenyl)propanol sulfamate ester

There total 2 articles about 3-(4-bromophenyl)propanol sulfamate ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 25574-11-2
3-(4-bromophenyl)propanol

: 1072126-72-7
3-(4-bromophenyl)propanol sulfamate ester

Guidance literature:: With pyridine; formic acid; isocyanate de chlorosulfonyle; In dichloromethane;
DOI:10.1002/anie.200801445

Reference yield: 68.0%

: 1072126-72-7
3-(4-bromophenyl)propanol sulfamate ester

Guidance literature:: With formic acid; isocyanate de chlorosulfonyle; triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield: 79.0%

: 1072126-72-7
3-(4-bromophenyl)propanol sulfamate ester

: (±)-4-(4-bromophenyl)-1,2,3-oxathiazinane 2,2-dioxide

Guidance literature:: With tert-Butyl hypoiodite; sodium iodide; In acetonitrile; at 20 ℃; Reagent/catalyst; Irradiation;
DOI:10.1039/c9cc06410a