C₁₂H₁₆O₄

Base Information

Chemical Name:C₁₂H₁₆O₄
CAS No.:1179989-35-5
Molecular Formula:C₁₂H₁₆O₄
Molecular Weight:224.257
Hs Code.:

C<sub>12</sub>H<sub>16</sub>O<sub>4</sub>

Synonyms:C₁₂H₁₆O₄

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Chemical Property of C₁₂H₁₆O₄

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Technology Process of C₁₂H₁₆O₄

There total 1 articles about C₁₂H₁₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1179989-34-4
C₂₀H₂₂O₆

: 1179989-35-5
C₁₂H₁₆O₄

Guidance literature:: With sodium methylate; In methanol;
DOI:10.1016/j.tetlet.2009.05.092

Reference yield:

: 1179989-35-5
C₁₂H₁₆O₄

: 1179989-36-6
C₁₂H₁₄O₄

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane;
DOI:10.1016/j.tetlet.2009.05.092

Reference yield:

: 1179989-35-5
C₁₂H₁₆O₄

: 1334288-70-8
C₂₇H₄₃IO₄Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 °C

2.1: potassium carbonate / methanol / 1.17 h / 0 - 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride / tetrahydrofuran / 0.33 h

4.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C

5.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1.5 h

6.1: tin(IV) chloride / dichloromethane / 0.75 h / -78 °C

6.2: 3 h / -78 °C

6.3: -78 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride; sulfur trioxide pyridine complex; tin(IV) chloride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; toluene; 6.1: Sakurai reaction / 6.2: Sakurai reaction;
DOI:10.1016/j.tet.2011.07.066