methyl 3-[4-(3-chloro-4-methoxybenzylamino)benzothieno-[2,3-d]pyrimidin-2-yl]propionate

Base Information

• Chemical Name: methyl 3-[4-(3-chloro-4-methoxybenzylamino)benzothieno-[2,3-d]pyrimidin-2-yl]propionate
• CAS No.: 247909-64-4
• Molecular Formula: C₂₂H₂₀ClN₃O₃S
• Molecular Weight: 441.938

Synonyms:methyl 3-[4-(3-chloro-4-methoxybenzylamino)benzothieno-[2,3-d]pyrimidin-2-yl]propionate

Chemical Property of methyl 3-[4-(3-chloro-4-methoxybenzylamino)benzothieno-[2,3-d]pyrimidin-2-yl]propionate

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Technology Process of methyl 3-[4-(3-chloro-4-methoxybenzylamino)benzothieno-[2,3-d]pyrimidin-2-yl]propionate

There total 3 articles about methyl 3-[4-(3-chloro-4-methoxybenzylamino)benzothieno-[2,3-d]pyrimidin-2-yl]propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Methyl 3-(4-chlorobenzothieno[2, 3-d]pyrimid in-2-yl)propionate (247909-63-3) + (3-chloro-4-methoxyphenyl)methanamine (115514-77-7) → methyl 3-[4-(3-chloro-4-methoxybenzylamino)benzothieno-[2,3-d]pyrimidin-2-yl]propionate (247909-64-4)

Guidance literature:

In 1-methyl-pyrrolidin-2-one; at 110 ℃; for 5h;

Reference yield:

Methyl 3-(4-chlorobenzothieno[2, 3-d]pyrimid in-2-yl)propionate (247909-63-3) + 3-cyano-propionic acid methyl ester (4107-62-4) + (3-chloro-4-methoxyphenyl)methanamine (115514-77-7) → methyl 3-[4-(3-chloro-4-methoxybenzylamino)benzothieno-[2,3-d]pyrimidin-2-yl]propionate (247909-64-4)

Guidance literature:

With hydrogen sulfide; dimethyl amine; trichlorophosphate; In 1-methyl-pyrrolidin-2-one;

Reference yield:

Methyl 3-(4-chlorobenzothieno[2, 3-d]pyrimid in-2-yl)propionate (247909-63-3) + 3-cyano-propionic acid methyl ester (4107-62-4) + (3-chloro-4-methoxyphenyl)methanamine (115514-77-7) → methyl 3-[4-(3-chloro-4-methoxybenzylamino)benzothieno-[2,3-d]pyrimidin-2-yl]propionate (247909-64-4) + methyl 2-(4-(3-chloro-4-methoxybenzylamino)benzothieno[2,3-d]-pyrimidin-2-yl)acetate

Guidance literature:

With hydrogen sulfide; dimethyl amine; trichlorophosphate; In 1-methyl-pyrrolidin-2-one;

upstream raw materials:

Methyl 3-(4-chlorobenzothieno[2, 3-d]pyrimid in-2-yl)propionate

(3-chloro-4-methoxyphenyl)methanamine

3-cyano-propionic acid methyl ester

Downstream raw materials:

3-[4-(3-chloro-4-methoxy-benzylamino)-benzo[4,5]thieno[2,3-d]pyrimidin-2-yl]-propionic acid

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