C₂₄H₃₇IO₅Si

Base Information

Chemical Name:C₂₄H₃₇IO₅Si
CAS No.:1388152-96-2
Molecular Formula:C₂₄H₃₇IO₅Si
Molecular Weight:560.545
Hs Code.:

C<sub>24</sub>H<sub>37</sub>IO<sub>5</sub>Si

Synonyms:C₂₄H₃₇IO₅Si

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Chemical Property of C₂₄H₃₇IO₅Si

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Technology Process of C₂₄H₃₇IO₅Si

There total 20 articles about C₂₄H₃₇IO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1388153-31-8
C₂₄H₃₅IO₅Si

: 1388152-96-2
C₂₄H₃₇IO₅Si

Guidance literature:: With 2-nitrobenzenesulfonyl hydrazide; triethylamine; In tetrahydrofuran; isopropyl alcohol; at 0 - 20 ℃; for 6.5h;
DOI:10.1021/ja305864z

Reference yield:

: C₂₆H₄₀O₆Si

: 1388152-96-2
C₂₄H₃₇IO₅Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 °C / Inert atmosphere

2.1: titanium(IV) isopropylate; (-)-diethyl tartrate / dichloromethane / 0.5 h / -20 °C / Molecular sieve

2.2: -20 °C / Molecular sieve

3.1: N-chloro-succinimide; triphenylphosphine; methyloxirane / dichloromethane / 0.75 h / 0 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 0.75 h / -40 °C / Inert atmosphere

5.1: N-iodo-succinimide; silver nitrate / acetone / 1 h / 0 °C

6.1: 2-nitrobenzenesulfonyl hydrazide; triethylamine / tetrahydrofuran; isopropyl alcohol / 6.5 h / 0 - 20 °C

With titanium(IV) isopropylate; N-chloro-succinimide; N-iodo-succinimide; (-)-diethyl tartrate; 2-nitrobenzenesulfonyl hydrazide; diisobutylaluminium hydride; silver nitrate; triethylamine; triphenylphosphine; methyloxirane; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; isopropyl alcohol; acetone; 2.1: Sharpless epoxidation / 2.2: Sharpless epoxidation;
DOI:10.1021/ja305864z

Reference yield:

: 1388153-25-0
C₂₇H₄₈O₅Si₂

: 1388152-96-2
C₂₄H₃₇IO₅Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: camphor-10-sulfonic acid / methanol; dichloromethane / 5 h / 0 °C

2.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

3.2: 2 h / -78 - 0 °C

4.1: tetrahydrofuran / 0.5 h / 20 °C

5.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C

6.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 1.5 h / 20 °C

6.2: 1 h / 20 °C

7.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 °C / Inert atmosphere

8.1: titanium(IV) isopropylate; (-)-diethyl tartrate / dichloromethane / 0.5 h / -20 °C / Molecular sieve

8.2: -20 °C / Molecular sieve

9.1: N-chloro-succinimide; triphenylphosphine; methyloxirane / dichloromethane / 0.75 h / 0 °C

10.1: lithium diisopropyl amide / tetrahydrofuran / 0.75 h / -40 °C / Inert atmosphere

11.1: N-iodo-succinimide; silver nitrate / acetone / 1 h / 0 °C

12.1: 2-nitrobenzenesulfonyl hydrazide; triethylamine / tetrahydrofuran; isopropyl alcohol / 6.5 h / 0 - 20 °C

With titanium(IV) isopropylate; N-chloro-succinimide; N-iodo-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; (-)-diethyl tartrate; camphor-10-sulfonic acid; 2-nitrobenzenesulfonyl hydrazide; potassium tert-butylate; dihydrogen peroxide; sulfur trioxide pyridine complex; diisobutylaluminium hydride; silver nitrate; triethylamine; triphenylphosphine; methyloxirane; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; isopropyl alcohol; acetone; 8.1: Sharpless epoxidation / 8.2: Sharpless epoxidation;
DOI:10.1021/ja305864z