10-(3,4-dimethoxyphenyl)-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxole-7,9-dione

Base Information

Chemical Name:10-(3,4-dimethoxyphenyl)-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxole-7,9-dione
CAS No.:1219694-00-4
Molecular Formula:C₂₁H₁₄O₇
Molecular Weight:378.338
Hs Code.:

Synonyms:10-(3,4-dimethoxyphenyl)-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxole-7,9-dione

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Chemical Property of 10-(3,4-dimethoxyphenyl)-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxole-7,9-dione

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Technology Process of 10-(3,4-dimethoxyphenyl)-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxole-7,9-dione

There total 2 articles about 10-(3,4-dimethoxyphenyl)-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxole-7,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-31-6
maleic anhydride

: 840529-31-9
(3,4-dimethoxy-phenyl)-(5-[1,3]dioxolan-2-yl-benzo[1,3]dioxol-4-yl)-methanol

: 1219694-00-4
10-(3,4-dimethoxyphenyl)-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxole-7,9-dione

Guidance literature:: With acetic anhydride; acetic acid; In dichloromethane; at 140 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.bmc.2009.12.038

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 1219694-00-4
10-(3,4-dimethoxyphenyl)-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxole-7,9-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere

1.2: 3 h / -78 - 20 °C / Inert atmosphere

2.1: acetic anhydride; acetic acid / dichloromethane / 24 h / 140 °C / Inert atmosphere

With n-butyllithium; acetic anhydride; acetic acid; In tetrahydrofuran; hexane; dichloromethane; 2.1: |Diels-Alder Cycloaddition;
DOI:10.1016/j.bmc.2012.11.037

Reference yield: 65.0%

: 1219694-00-4
10-(3,4-dimethoxyphenyl)-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxole-7,9-dione

: 10-(3,4-dimethoxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

Guidance literature:: 10-(3,4-dimethoxyphenyl)-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxole-7,9-dione; With sodium tetrahydroborate; In tetrahydrofuran; at 20 ℃; under 760.051 Torr; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; under 760.051 Torr; Inert atmosphere;
DOI:10.1016/j.bmc.2009.12.038