Silber-(diazomethyl)-diphenylphosphinoxid

Base Information

Chemical Name:Silber-(diazomethyl)-diphenylphosphinoxid
CAS No.:70550-76-4
Molecular Formula:C₁₃H₁₀AgN₂OP
Molecular Weight:349.077
Hs Code.:

Synonyms:Silber-(diazomethyl)-diphenylphosphinoxid

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Chemical Property of Silber-(diazomethyl)-diphenylphosphinoxid

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Technology Process of Silber-(diazomethyl)-diphenylphosphinoxid

There total 1 articles about Silber-(diazomethyl)-diphenylphosphinoxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20667-12-3
silver(l) oxide

: 5353-66-2
diphenylphosphorylazide

: 70550-76-4
Silber-(diazomethyl)-diphenylphosphinoxid

Guidance literature:: With magnesium sulfate; In chloroform; molar ratio Ag2O:diazo compound=1:2, stirring with MgSO4 in the dark, evapn. in vac.;; recrystn. from acetone/CHCl3;;

Reference yield: 94.0%

: tropylium bromide

: 70550-76-4
Silber-(diazomethyl)-diphenylphosphinoxid

: 70550-81-1
<(1,3,5-Cycloheptatrien-7-yl)diazomethyl>diphenylphosphanoxid

Guidance literature:: In dichloromethane; at 0 ℃; for 1.5h;

Reference yield: 90.0%

: Cp*2Rh₂(CO)2

: 70550-76-4
Silber-(diazomethyl)-diphenylphosphinoxid

: di-μ-carbonyl-μ-[diazo(diphenylphosphinyl)methylsilver-Ag]bis[(η5-pentamethylcyclopentadienyl)rhodium](Rh-Rh)

Guidance literature:: In dichloromethane; -78 °C, warming to room temp. for 2 h; evapn. of the solvent in vac., crystn. of the residue from dichloromethane/diethyl ether at -35 °C, elem. anal.;