benzyl 1-((2-chloroallyl)(isobutyl)amino)-1-oxopent-4-en-2-ylcarbamate

Base Information

Chemical Name:benzyl 1-((2-chloroallyl)(isobutyl)amino)-1-oxopent-4-en-2-ylcarbamate
CAS No.:1617532-18-9
Molecular Formula:C₂₀H₂₇ClN₂O₃
Molecular Weight:378.899
Hs Code.:

Synonyms:benzyl 1-((2-chloroallyl)(isobutyl)amino)-1-oxopent-4-en-2-ylcarbamate

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Chemical Property of benzyl 1-((2-chloroallyl)(isobutyl)amino)-1-oxopent-4-en-2-ylcarbamate

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Technology Process of benzyl 1-((2-chloroallyl)(isobutyl)amino)-1-oxopent-4-en-2-ylcarbamate

There total 1 articles about benzyl 1-((2-chloroallyl)(isobutyl)amino)-1-oxopent-4-en-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 133773-64-5
(RS)-N-(benzyloxycarbonyl)-2-amino-4-pentenoic acid

: (2-Chloro-allyl)-isobutyl-amine

: 1617532-18-9
benzyl 1-((2-chloroallyl)(isobutyl)amino)-1-oxopent-4-en-2-ylcarbamate

Guidance literature:: (RS)-N-(benzyloxycarbonyl)-2-amino-4-pentenoic acid; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; at -15 ℃; for 0.5h;

(2-Chloro-allyl)-isobutyl-amine; at 20 ℃;
DOI:10.1021/ol501529z

Reference yield: 85.0%

: 1617532-18-9
benzyl 1-((2-chloroallyl)(isobutyl)amino)-1-oxopent-4-en-2-ylcarbamate

: 1617532-24-7
benzyl 6-chloro-1-isobutyl-2-oxo-2,3,4,7-tetrahydro-1H-azepin-3-ylcarbamate

Guidance literature:: With [1,3-bis(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro-(3-phenyl-1H-inden-1-ylidene)(tricyclohexylphosphine)ruthenium(II); In dichloromethane; at 65 ℃;
DOI:10.1021/ol501529z

Reference yield:

: 1617532-18-9
benzyl 1-((2-chloroallyl)(isobutyl)amino)-1-oxopent-4-en-2-ylcarbamate

: 4-isobutyl-6-(benzyloxycarbonylamino)-12-oxa-4-azatricyclo[7.2.1.0^2,8]dodeca-2,10-dien-5-one

Guidance literature:: Multi-step reaction with 2 steps

1: [1,3-bis(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro-(3-phenyl-1H-inden-1-ylidene)(tricyclohexylphosphine)ruthenium(II) / dichloromethane / 65 °C

2: potassium tert-butylate / 20 °C

With [1,3-bis(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro-(3-phenyl-1H-inden-1-ylidene)(tricyclohexylphosphine)ruthenium(II); potassium tert-butylate; In dichloromethane; 2: |Diels-Alder Cycloaddition;
DOI:10.1021/ol501529z