(3S,4S,8S,9S)-3,4,8,9-Tetraethoxy-1,6-bis-(toluene-4-sulfonyl)-[1,6]diazecane

Base Information

Chemical Name:(3S,4S,8S,9S)-3,4,8,9-Tetraethoxy-1,6-bis-(toluene-4-sulfonyl)-[1,6]diazecane
CAS No.:123529-98-6
Molecular Formula:C₃₀H₄₆N₂O₈S₂
Molecular Weight:626.836
Hs Code.:

Synonyms:(3S,4S,8S,9S)-3,4,8,9-Tetraethoxy-1,6-bis-(toluene-4-sulfonyl)-[1,6]diazecane

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Chemical Property of (3S,4S,8S,9S)-3,4,8,9-Tetraethoxy-1,6-bis-(toluene-4-sulfonyl)-[1,6]diazecane

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Technology Process of (3S,4S,8S,9S)-3,4,8,9-Tetraethoxy-1,6-bis-(toluene-4-sulfonyl)-[1,6]diazecane

There total 5 articles about (3S,4S,8S,9S)-3,4,8,9-Tetraethoxy-1,6-bis-(toluene-4-sulfonyl)-[1,6]diazecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 123530-01-8
C₂₂H₃₀O₈S₂

: 123530-03-0
C₂₂H₃₂N₂O₆S₂

: 123529-98-6
(3S,4S,8S,9S)-3,4,8,9-Tetraethoxy-1,6-bis-(toluene-4-sulfonyl)-[1,6]diazecane

: (3S,4S,8S,9S,13S,14S,18S,19S)-3,4,8,9,13,14,18,19-Octaethoxy-1,6,11,16-tetrakis-(toluene-4-sulfonyl)-1,6,11,16-tetraaza-cycloicosane

Guidance literature:: With sodium ethanolate; In N,N-dimethyl-formamide; at 95 - 100 ℃;
DOI:10.1246/cl.1989.283

Reference yield:

: 123555-85-1
dimethyl (O,O'-diethyl)-D-tartrate

: 123529-98-6
(3S,4S,8S,9S)-3,4,8,9-Tetraethoxy-1,6-bis-(toluene-4-sulfonyl)-[1,6]diazecane

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄

3: 20 percent / NaOEt / dimethylformamide / 95 - 100 °C

With lithium aluminium tetrahydride; sodium ethanolate; In N,N-dimethyl-formamide;
DOI:10.1246/cl.1989.283

Reference yield:

: 123530-00-7
(2S,3S)-2,3-Diethoxy-butane-1,4-diol

: 123529-98-6
(3S,4S,8S,9S)-3,4,8,9-Tetraethoxy-1,6-bis-(toluene-4-sulfonyl)-[1,6]diazecane

Guidance literature:: Multi-step reaction with 2 steps

2: 20 percent / NaOEt / dimethylformamide / 95 - 100 °C

With sodium ethanolate; In N,N-dimethyl-formamide;
DOI:10.1246/cl.1989.283