3-[4-(15-oxo-2,3,5,6,8,9-hexahydro-15H-[1,4,7,10]tetraoxacyclododecino[2,3-h]chromen-14-yl)phenoxy]phthalonitrile

Base Information

Chemical Name:3-[4-(15-oxo-2,3,5,6,8,9-hexahydro-15H-[1,4,7,10]tetraoxacyclododecino[2,3-h]chromen-14-yl)phenoxy]phthalonitrile
CAS No.:1392240-38-8
Molecular Formula:C₂₉H₂₂N₂O₇
Molecular Weight:510.503
Hs Code.:

Synonyms:3-[4-(15-oxo-2,3,5,6,8,9-hexahydro-15H-[1,4,7,10]tetraoxacyclododecino[2,3-h]chromen-14-yl)phenoxy]phthalonitrile

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Chemical Property of 3-[4-(15-oxo-2,3,5,6,8,9-hexahydro-15H-[1,4,7,10]tetraoxacyclododecino[2,3-h]chromen-14-yl)phenoxy]phthalonitrile

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Technology Process of 3-[4-(15-oxo-2,3,5,6,8,9-hexahydro-15H-[1,4,7,10]tetraoxacyclododecino[2,3-h]chromen-14-yl)phenoxy]phthalonitrile

There total 4 articles about 3-[4-(15-oxo-2,3,5,6,8,9-hexahydro-15H-[1,4,7,10]tetraoxacyclododecino[2,3-h]chromen-14-yl)phenoxy]phthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 1360589-55-4
7,8-dihydroxy-3-[p-(2',3'-dicyanophenoxy)phenyl]coumarin

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 1392240-38-8
3-[4-(15-oxo-2,3,5,6,8,9-hexahydro-15H-[1,4,7,10]tetraoxacyclododecino[2,3-h]chromen-14-yl)phenoxy]phthalonitrile

Guidance literature:: With sodium carbonate; In acetonitrile; for 72h; Reflux; Inert atmosphere;
DOI:10.1016/j.jphotochem.2011.06.007

Reference yield:

: 1193356-71-6
4-(2,3-dicyanophenoxy)phenylacetic acid

: 1392240-38-8
3-[4-(15-oxo-2,3,5,6,8,9-hexahydro-15H-[1,4,7,10]tetraoxacyclododecino[2,3-h]chromen-14-yl)phenoxy]phthalonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: acetic anhydride / 8 h / 160 - 170 °C / Inert atmosphere

2: hydrogenchloride / water / 18 h / 60 °C / pH 3 / Inert atmosphere

3: sodium carbonate / acetonitrile / 72 h / Reflux; Inert atmosphere

With hydrogenchloride; sodium carbonate; In water; acetic anhydride; acetonitrile;
DOI:10.1016/j.jphotochem.2011.06.007

Reference yield:

: 7,8-diacetoxy-3-[p-(2,3-dicyanophenoxy)phenyl]coumarin

: 1392240-38-8
3-[4-(15-oxo-2,3,5,6,8,9-hexahydro-15H-[1,4,7,10]tetraoxacyclododecino[2,3-h]chromen-14-yl)phenoxy]phthalonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water / 18 h / 60 °C / pH 3 / Inert atmosphere

2: sodium carbonate / acetonitrile / 72 h / Reflux; Inert atmosphere

With hydrogenchloride; sodium carbonate; In water; acetonitrile;
DOI:10.1016/j.jphotochem.2011.06.007