2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-glucopyranosyl-(1'->3'')-2''-O-[D7]benzyl-4'',6''-O-cyclohexylidene-α-D-mannopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-α-D-glucopyranosid-2-yl) acetal

Base Information

• Chemical Name: 2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-glucopyranosyl-(1'->3'')-2''-O-[D7]benzyl-4'',6''-O-cyclohexylidene-α-D-mannopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-α-D-glucopyranosid-2-yl) acetal
• CAS No.: 1075709-00-0
• Molecular Formula: C₉₅H₁₁₄O₂₂S
• Molecular Weight: 1667.78

Synonyms:2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-glucopyranosyl-(1'->3'')-2''-O-[D7]benzyl-4'',6''-O-cyclohexylidene-α-D-mannopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-α-D-glucopyranosid-2-yl) acetal

Chemical Property of 2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-glucopyranosyl-(1'->3'')-2''-O-[D7]benzyl-4'',6''-O-cyclohexylidene-α-D-mannopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-α-D-glucopyranosid-2-yl) acetal

Chemical Property:

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• Pictogram(s):  
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Technology Process of 2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-glucopyranosyl-(1'->3'')-2''-O-[D7]benzyl-4'',6''-O-cyclohexylidene-α-D-mannopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-α-D-glucopyranosid-2-yl) acetal

There total 2 articles about 2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-glucopyranosyl-(1'->3'')-2''-O-[D7]benzyl-4'',6''-O-cyclohexylidene-α-D-mannopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-α-D-glucopyranosid-2-yl) acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-β-D-glucopyranoside (1075708-69-8) + 4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-2-O-(2-naphthylmethyl)-α-D-glucopyranosyl-(1->3)-2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3)-2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-mannopyranoside (1075708-99-4) → 2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-glucopyranosyl-(1'->3'')-2''-O-[D7]benzyl-4'',6''-O-cyclohexylidene-α-D-mannopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-α-D-glucopyranosid-2-yl) acetal (1075709-00-0)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 15h; Inert atmosphere; Molecular sieve;

DOI:10.1002/ejoc.200800249

Reference yield: 50.0%

4-methoxyphenyl 3-O-(benzyl-d7)-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3)-2-O-(benzyl-d7)-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3)-2-O-(benzyl-d7)-4,6-O-cyclohexylidene-α-D-mannopyranoside + methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-2-O-2-naphthylmethyl-1-thio-β-D-glucopyranoside (1075708-62-1) → 2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-glucopyranosyl-(1'->3'')-2''-O-[D7]benzyl-4'',6''-O-cyclohexylidene-α-D-mannopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-α-D-glucopyranosid-2-yl) acetal (1075709-00-0)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 20h; Inert atmosphere; Molecular sieve;

DOI:10.1002/ejoc.200800249

Reference yield: 77.0%

2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-glucopyranosyl-(1'->3'')-2''-O-[D7]benzyl-4'',6''-O-cyclohexylidene-α-D-mannopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-α-D-glucopyranosid-2-yl) acetal (1075709-00-0) → 4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->2)-3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3)-2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3)-2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-mannopyranoside (1075708-80-3)

Guidance literature:

2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-glucopyranosyl-(1'->3'')-2''-O-[D7]benzyl-4'',6''-O-cyclohexylidene-α-D-mannopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-α-D-glucopyranosid-2-yl) acetal; With 2,6-di-tert-butyl-4-methylpyridine; tris-(trimethylsilyl)silane; methyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 20 ℃; for 14h; Molecular sieve; Inert atmosphere;

With sodium hydrogencarbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,2-dichloro-ethane; at 20 ℃; for 5h;

DOI:10.1002/ejoc.200800249

upstream raw materials:

methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-2-O-2-naphthylmethyl-1-thio-β-D-glucopyranoside

methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-β-D-glucopyranoside

4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-2-O-(2-naphthylmethyl)-α-D-glucopyranosyl-(1->3)-2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3)-2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-mannopyranoside

Downstream raw materials:

4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->2)-3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3)-2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3)-2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-mannopyranoside

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