N'-methyl-N'-(1H-tetrazol-5-ylmethyl)-hydrazinecarboxylic acid benzyl ester

Base Information

Chemical Name:N'-methyl-N'-(1H-tetrazol-5-ylmethyl)-hydrazinecarboxylic acid benzyl ester
CAS No.:604003-93-2
Molecular Formula:C₁₁H₁₄N₆O₂
Molecular Weight:262.271
Hs Code.:

<i>N</i>'-methyl-<i>N</i>'-(1<i>H</i>-tetrazol-5-ylmethyl)-hydrazinecarboxylic acid benzyl ester

Synonyms:N'-methyl-N'-(1H-tetrazol-5-ylmethyl)-hydrazinecarboxylic acid benzyl ester

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Chemical Property of N'-methyl-N'-(1H-tetrazol-5-ylmethyl)-hydrazinecarboxylic acid benzyl ester

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Technology Process of N'-methyl-N'-(1H-tetrazol-5-ylmethyl)-hydrazinecarboxylic acid benzyl ester

There total 4 articles about N'-methyl-N'-(1H-tetrazol-5-ylmethyl)-hydrazinecarboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 604003-92-1
N'-cyanomethyl-N'-methyl-hydrazinecarboxylic acid benzyl ester

: 604003-93-2
N'-methyl-N'-(1H-tetrazol-5-ylmethyl)-hydrazinecarboxylic acid benzyl ester

Guidance literature:: With azido tributyltin (IV); at 110 ℃; for 72h;
DOI:10.1016/S0960-894X(03)00393-7

Reference yield:

: 57699-92-0
2-benzyl 1-tert-butyl 1-methylhydrazine-1,2-dicarboxylate

: 604003-93-2
N'-methyl-N'-(1H-tetrazol-5-ylmethyl)-hydrazinecarboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / HCl / dioxane / 4 h / 20 °C

2: 87 percent / dimethylformamide / 14 h / 20 °C

3: 83 percent / Bu₃SnN₃ / 72 h / 110 °C

With hydrogenchloride; azido tributyltin (IV); In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(03)00393-7

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 604003-93-2
N'-methyl-N'-(1H-tetrazol-5-ylmethyl)-hydrazinecarboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / NaHCO₃ / ethyl acetate / 1 h / 0 - 1 °C

2: 100 percent / HCl / dioxane / 4 h / 20 °C

3: 87 percent / dimethylformamide / 14 h / 20 °C

4: 83 percent / Bu₃SnN₃ / 72 h / 110 °C

With hydrogenchloride; sodium hydrogencarbonate; azido tributyltin (IV); In 1,4-dioxane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(03)00393-7