benzyl-(2S)-2-[(R)-1-acetoxy-2-oxo-1-(phenethyl)prop-3-ylcarbamoyl]-4-oxopyrrolidinedine-1-carboxylate

Base Information

• Chemical Name: benzyl-(2S)-2-[(R)-1-acetoxy-2-oxo-1-(phenethyl)prop-3-ylcarbamoyl]-4-oxopyrrolidinedine-1-carboxylate
• CAS No.: 1162084-58-3
• Molecular Formula: C₂₆H₂₈N₂O₇
• Molecular Weight: 480.518

Synonyms:benzyl-(2S)-2-[(R)-1-acetoxy-2-oxo-1-(phenethyl)prop-3-ylcarbamoyl]-4-oxopyrrolidinedine-1-carboxylate

Chemical Property of benzyl-(2S)-2-[(R)-1-acetoxy-2-oxo-1-(phenethyl)prop-3-ylcarbamoyl]-4-oxopyrrolidinedine-1-carboxylate

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Technology Process of benzyl-(2S)-2-[(R)-1-acetoxy-2-oxo-1-(phenethyl)prop-3-ylcarbamoyl]-4-oxopyrrolidinedine-1-carboxylate

There total 1 articles about benzyl-(2S)-2-[(R)-1-acetoxy-2-oxo-1-(phenethyl)prop-3-ylcarbamoyl]-4-oxopyrrolidinedine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C13H17NO3*ClH (1162084-40-3) + 1-benzyloxycarbonyl-4-keto-L-proline (64187-47-9) → benzyl-(2S)-2-[(R)-1-acetoxy-2-oxo-1-(phenethyl)prop-3-ylcarbamoyl]-4-oxopyrrolidinedine-1-carboxylate (1162084-58-3)

Guidance literature:

1-benzyloxycarbonyl-4-keto-L-proline; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 1.5h; Inert atmosphere;

C₁₃H₁₇NO₃*ClH; With triethylamine; In dichloromethane; at 20 ℃; for 1.5h; Inert atmosphere;

DOI:10.1515/znb-2008-1108

Reference yield: 70.0%

benzyl-(2S)-2-[(R)-1-acetoxy-2-oxo-1-(phenethyl)prop-3-ylcarbamoyl]-4-oxopyrrolidinedine-1-carboxylate (1162084-58-3) → benzyl-(2S)-2-[(R)-1-hydroxy-2-oxo-1-(phenethyl)prop-3-ylcarbamoyl]-4-oxopyrrolidinedine-1-carboxylate (1162084-64-1)

Guidance literature:

With water; potassium carbonate; In methanol; dichloromethane; at -10 - 0 ℃; for 0.5h;

DOI:10.1515/znb-2008-1108

upstream raw materials:

C₁₃H₁₇NO₃*ClH

1-benzyloxycarbonyl-4-keto-L-proline

Downstream raw materials:

benzyl-(2S)-2-[(R)-1-hydroxy-2-oxo-1-(phenethyl)prop-3-ylcarbamoyl]-4-oxopyrrolidinedine-1-carboxylate

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