Technology Process of C40H53N5O13S
There total 8 articles about C40H53N5O13S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C31H42N4O11S;
With
4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
for 1h;
3,4,5-Trimethoxyaniline;
In
dichloromethane;
for 12h;
DOI:10.1016/j.bmcl.2011.04.070
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine / 1,4-dioxane; water / 0 - 20 °C
2.1: triethylamine / acetonitrile / 7 h / 20 °C
3.1: triethylamine / dichloromethane / 3 h / 20 °C
4.1: lithium hydroxide / tetrahydrofuran; water / 4 h / 20 °C
5.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 20 °C
5.2: 12 h
With
4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmcl.2011.04.070
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium hydroxide / tetrahydrofuran; water / 4 h / 20 °C
2.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 20 °C
2.2: 12 h
With
4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmcl.2011.04.070
