2-acetyl-3-(3-methoxycarbonylprop-2-enyl)-1,4-dimethoxybenzene

Base Information

• Chemical Name: 2-acetyl-3-(3-methoxycarbonylprop-2-enyl)-1,4-dimethoxybenzene
• CAS No.: 78572-97-1
• Molecular Formula: C₁₅H₁₈O₅
• Molecular Weight: 278.305
• Mol file: 78572-97-1.mol

Synonyms:2-acetyl-3-(3-methoxycarbonylprop-2-enyl)-1,4-dimethoxybenzene

Chemical Property of 2-acetyl-3-(3-methoxycarbonylprop-2-enyl)-1,4-dimethoxybenzene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-acetyl-3-(3-methoxycarbonylprop-2-enyl)-1,4-dimethoxybenzene

There total 3 articles about 2-acetyl-3-(3-methoxycarbonylprop-2-enyl)-1,4-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

2-acetyl-3-formylmethyl-1,4-dimethoxybenzene (78572-96-0) + methyl (triphenylphosphoranylidene)acetate (21204-67-1,2605-67-6) → 2-acetyl-3-(3-methoxycarbonylprop-2-enyl)-1,4-dimethoxybenzene (78572-97-1)

Guidance literature:

In benzene; for 24h; Ambient temperature;

DOI:10.1039/P19810001191

Reference yield:

4,7-dimethoxyindan-1-one (52428-09-8) → 2-acetyl-3-(3-methoxycarbonylprop-2-enyl)-1,4-dimethoxybenzene (78572-97-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 2.) 10percent hydrochloric acid / 1.) ether, room temperature, 1 h, 2.) 2 min

2: 1.) osmium tetraoxide, 2.) sodium metaperiodate / 1.) dimethoxyethane, water, room temperature, 5 min, 2.) 4 h

3: 45 percent / benzene / 24 h / Ambient temperature

With hydrogenchloride; sodium periodate; osmium(VIII) oxide; In benzene;

DOI:10.1039/P19810001191

Reference yield:

4,7-dimethoxy-3-methylindene (78572-95-9) → 2-acetyl-3-(3-methoxycarbonylprop-2-enyl)-1,4-dimethoxybenzene (78572-97-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) osmium tetraoxide, 2.) sodium metaperiodate / 1.) dimethoxyethane, water, room temperature, 5 min, 2.) 4 h

2: 45 percent / benzene / 24 h / Ambient temperature

With sodium periodate; osmium(VIII) oxide; In benzene;

DOI:10.1039/P19810001191

upstream raw materials:

2-acetyl-3-formylmethyl-1,4-dimethoxybenzene

methyl (triphenylphosphoranylidene)acetate

4,7-dimethoxyindan-1-one

4,7-dimethoxy-3-methylindene