(S)-4-(4-aminomethyl-phenoxy)-2-tert-butoxycarbonylamino-butyric acid cyclopentyl ester

Base Information

Chemical Name:(S)-4-(4-aminomethyl-phenoxy)-2-tert-butoxycarbonylamino-butyric acid cyclopentyl ester
CAS No.:914452-43-0
Molecular Formula:C₂₁H₃₂N₂O₅
Molecular Weight:392.495
Hs Code.:

Synonyms:(S)-4-(4-aminomethyl-phenoxy)-2-tert-butoxycarbonylamino-butyric acid cyclopentyl ester

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Chemical Property of (S)-4-(4-aminomethyl-phenoxy)-2-tert-butoxycarbonylamino-butyric acid cyclopentyl ester

Chemical Property:

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Technology Process of (S)-4-(4-aminomethyl-phenoxy)-2-tert-butoxycarbonylamino-butyric acid cyclopentyl ester

There total 7 articles about (S)-4-(4-aminomethyl-phenoxy)-2-tert-butoxycarbonylamino-butyric acid cyclopentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 914382-63-1
(S)-2-tert-butoxycarbonylamino-4-(tert-butyl-dimethyl-silanyloxy)-butyric acid cyclopentyl ester

: 914452-43-0
(S)-4-(4-aminomethyl-phenoxy)-2-tert-butoxycarbonylamino-butyric acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: water; acetic acid / tetrahydrofuran / 16 h / 30 °C

2: pyridine; N-Bromosuccinimide; triphenylphosphine / dichloromethane / 18.08 h

3: potassium carbonate / N,N-dimethyl-formamide / 18 h / 50 °C

4: hydrogen / palladium on activated charcoal / ethyl acetate / 2 h

With pyridine; N-Bromosuccinimide; water; hydrogen; potassium carbonate; acetic acid; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 914382-65-3
(S)-4-bromo-2-tert-butoxycarbonylamino-butyric acid cyclopentyl ester

: 914452-43-0
(S)-4-(4-aminomethyl-phenoxy)-2-tert-butoxycarbonylamino-butyric acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 50 °C

2: hydrogen / palladium on activated charcoal / ethyl acetate / 2 h

With hydrogen; potassium carbonate; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 914382-64-2
(S)-2-tert-butoxycarbonylamino-4-hydroxy-butyric acid cyclopentyl ester

: 914452-43-0
(S)-4-(4-aminomethyl-phenoxy)-2-tert-butoxycarbonylamino-butyric acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; N-Bromosuccinimide; triphenylphosphine / dichloromethane / 18.08 h

2: potassium carbonate / N,N-dimethyl-formamide / 18 h / 50 °C

3: hydrogen / palladium on activated charcoal / ethyl acetate / 2 h

With pyridine; N-Bromosuccinimide; hydrogen; potassium carbonate; triphenylphosphine; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;