2-[2-(2-fluoromethylphenylsulfanyl)ethyl]-[1,3]dioxolane

Base Information

Chemical Name:2-[2-(2-fluoromethylphenylsulfanyl)ethyl]-[1,3]dioxolane
CAS No.:758717-02-1
Molecular Formula:C₁₂H₁₅FO₂S
Molecular Weight:242.314
Hs Code.:

Synonyms:2-[2-(2-fluoromethylphenylsulfanyl)ethyl]-[1,3]dioxolane

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Chemical Property of 2-[2-(2-fluoromethylphenylsulfanyl)ethyl]-[1,3]dioxolane

Chemical Property:

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Technology Process of 2-[2-(2-fluoromethylphenylsulfanyl)ethyl]-[1,3]dioxolane

There total 3 articles about 2-[2-(2-fluoromethylphenylsulfanyl)ethyl]-[1,3]dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4521-31-7
o-hydroxymethyl thiophenol

: 758717-02-1
2-[2-(2-fluoromethylphenylsulfanyl)ethyl]-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: methanesulfonyl chloride; triethylamine / tetrahydrofuran / 120 h

3: potassium fluoride; K[18F]-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]-hexacosane complex / acetonitrile / 0.5 h / 70 °C

With potassium fluoride; K[18F]-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]-hexacosane complex; potassium carbonate; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 758717-00-9
[2-(2-[1,3]dioxolan-2-ylethylsulfanyl)phenyl]methanol

: 758717-02-1
2-[2-(2-fluoromethylphenylsulfanyl)ethyl]-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonyl chloride; triethylamine / tetrahydrofuran / 120 h

2: potassium fluoride; K[18F]-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]-hexacosane complex / acetonitrile / 0.5 h / 70 °C

With potassium fluoride; K[18F]-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]-hexacosane complex; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; acetonitrile;

Reference yield:

: 18742-02-4
2-bromo-2-(2-ethyl)dioxolane

: 758717-02-1
2-[2-(2-fluoromethylphenylsulfanyl)ethyl]-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: methanesulfonyl chloride; triethylamine / tetrahydrofuran / 120 h

3: potassium fluoride; K[18F]-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]-hexacosane complex / acetonitrile / 0.5 h / 70 °C

With potassium fluoride; K[18F]-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]-hexacosane complex; potassium carbonate; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;