methyl (Z)-2-(2-nitrophenylhydrazono)-D-arabino-hexulosonate

Base Information

• Chemical Name: methyl (Z)-2-(2-nitrophenylhydrazono)-D-arabino-hexulosonate
• CAS No.: 239083-69-3
• Molecular Formula: C₁₃H₁₇N₃O₈
• Molecular Weight: 343.293

Synonyms:methyl (Z)-2-(2-nitrophenylhydrazono)-D-arabino-hexulosonate

Chemical Property of methyl (Z)-2-(2-nitrophenylhydrazono)-D-arabino-hexulosonate

Chemical Property:

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Technology Process of methyl (Z)-2-(2-nitrophenylhydrazono)-D-arabino-hexulosonate

There total 1 articles about methyl (Z)-2-(2-nitrophenylhydrazono)-D-arabino-hexulosonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(2-nitrophenyl)hydrazine (3034-19-3) + methyl β-D-arabino-hex-2-ulopyranosonate (72933-34-7) → methyl (Z)-2-(2-nitrophenylhydrazono)-D-arabino-hexulosonate (239083-69-3)

Guidance literature:

With hydrogenchloride; In methanol; for 1h; Heating;

DOI:10.1002/jhet.5570360302

Reference yield: 92.0%

methyl (Z)-2-(2-nitrophenylhydrazono)-D-arabino-hexulosonate (239083-69-3) → methyl (Z)-2-(2-aminophenylhydrazono)-D-arabino-hexulosonate

Guidance literature:

With hydrogen; platinum on activated charcoal; In methanol; under 760 Torr; Ambient temperature;

DOI:10.1002/jhet.5570360302

Reference yield:

methyl (Z)-2-(2-nitrophenylhydrazono)-D-arabino-hexulosonate (239083-69-3) → (E)-2-(2-nitrophenylhydrazono)-D-arabino-hexulosonic acid + (Z)-2-(2-nitrophenylhydrazono)-D-arabino-hexulosonic acid

Guidance literature:

With sodium hydroxide; for 0.166667h; Yield given;

DOI:10.1002/jhet.5570360302

upstream raw materials:

(2-nitrophenyl)hydrazine

methyl β-D-arabino-hex-2-ulopyranosonate

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