trans-2-(4-cyanocyclohexyl)-2-(3,3,3-trifluoropropylsulfonyl)acetnitrile

Base Information

Chemical Name:trans-2-(4-cyanocyclohexyl)-2-(3,3,3-trifluoropropylsulfonyl)acetnitrile
CAS No.:1097630-47-1
Molecular Formula:C₁₂H₁₅F₃N₂O₂S
Molecular Weight:308.325
Hs Code.:

Synonyms:trans-2-(4-cyanocyclohexyl)-2-(3,3,3-trifluoropropylsulfonyl)acetnitrile

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Chemical Property of trans-2-(4-cyanocyclohexyl)-2-(3,3,3-trifluoropropylsulfonyl)acetnitrile

Chemical Property:

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Technology Process of trans-2-(4-cyanocyclohexyl)-2-(3,3,3-trifluoropropylsulfonyl)acetnitrile

There total 4 articles about trans-2-(4-cyanocyclohexyl)-2-(3,3,3-trifluoropropylsulfonyl)acetnitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1300632-24-9
C₁₂H₁₃F₃N₂O₂S

: 1097630-47-1
trans-2-(4-cyanocyclohexyl)-2-(3,3,3-trifluoropropylsulfonyl)acetnitrile

: 1097630-46-0
cis-2-(4-cyanocyclohexyl)-2-(3,3,3-trifluoropropylsulfonyl)acetnitrile

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; at 0 - 20 ℃; for 6h;

Reference yield:

: 1086602-99-4
2-(3,3,3-trifluoropropylthio)acetonitrile

: 1097630-47-1
trans-2-(4-cyanocyclohexyl)-2-(3,3,3-trifluoropropylsulfonyl)acetnitrile

: 1097630-46-0
cis-2-(4-cyanocyclohexyl)-2-(3,3,3-trifluoropropylsulfonyl)acetnitrile

Guidance literature:: Multi-step reaction with 3 steps

1: dihydrogen peroxide / sodium tungstate (VI) dihydrate / water / 1 h / 65 - 70 °C

2: rac-Pro-OH / tetrahydrofuran / 6 h / Reflux

3: sodium tetrahydroborate / tetrahydrofuran / 6 h / 0 - 20 °C

With sodium tetrahydroborate; dihydrogen peroxide; rac-Pro-OH; sodium tungstate (VI) dihydrate; In tetrahydrofuran; water;

Reference yield:

: 1097630-65-3
S-(3,3,3-trifluoropropyl)ethanethioate

: 1097630-47-1
trans-2-(4-cyanocyclohexyl)-2-(3,3,3-trifluoropropylsulfonyl)acetnitrile

: 1097630-46-0
cis-2-(4-cyanocyclohexyl)-2-(3,3,3-trifluoropropylsulfonyl)acetnitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium methylate / tetrahydrofuran; methanol / 1.25 h / 0 - 20 °C

1.2: 3 h / 0 - 20 °C

2.1: dihydrogen peroxide / sodium tungstate (VI) dihydrate / water / 1 h / 65 - 70 °C

3.1: rac-Pro-OH / tetrahydrofuran / 6 h / Reflux

4.1: sodium tetrahydroborate / tetrahydrofuran / 6 h / 0 - 20 °C

With sodium tetrahydroborate; dihydrogen peroxide; sodium methylate; rac-Pro-OH; sodium tungstate (VI) dihydrate; In tetrahydrofuran; methanol; water;