1-(aminomethyl)-3,5-bis[(4,6-dimethylpyridin-2-yl)aminomethyl]-2,4,6-triethylbenzene

Base Information

• Chemical Name: 1-(aminomethyl)-3,5-bis[(4,6-dimethylpyridin-2-yl)aminomethyl]-2,4,6-triethylbenzene
• CAS No.: 1030362-70-9
• Molecular Formula: C₂₉H₄₁N₅
• Molecular Weight: 459.678
• Mol file: 1030362-70-9.mol

Synonyms:1-(aminomethyl)-3,5-bis[(4,6-dimethylpyridin-2-yl)aminomethyl]-2,4,6-triethylbenzene

Chemical Property of 1-(aminomethyl)-3,5-bis[(4,6-dimethylpyridin-2-yl)aminomethyl]-2,4,6-triethylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(aminomethyl)-3,5-bis[(4,6-dimethylpyridin-2-yl)aminomethyl]-2,4,6-triethylbenzene

There total 3 articles about 1-(aminomethyl)-3,5-bis[(4,6-dimethylpyridin-2-yl)aminomethyl]-2,4,6-triethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1-(bromomethyl)-3,5-bis[((4,6-dimethylpyridin-2-yl)amino)-methyl]-2,4,6-triethylbenzene → 1-(aminomethyl)-3,5-bis[(4,6-dimethylpyridin-2-yl)aminomethyl]-2,4,6-triethylbenzene (1030362-70-9)

Guidance literature:

With ammonia; In methanol; for 48h;

DOI:10.1055/s-2016-1561449

Reference yield:

2-Amino-4,6-dimethylpyridine (5407-87-4) → 1-(aminomethyl)-3,5-bis[(4,6-dimethylpyridin-2-yl)aminomethyl]-2,4,6-triethylbenzene (1030362-70-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / tetrahydrofuran; acetonitrile / 72 h / 20 °C

2: ammonia / water / 12 h

With ammonia; potassium carbonate; In tetrahydrofuran; water; acetonitrile;

DOI:10.1039/c0ob00960a

Reference yield:

1,3,5-tris(bromomethyl)-2,4,6-triethylbenzene (181058-08-2) → 1-(aminomethyl)-3,5-bis[(4,6-dimethylpyridin-2-yl)aminomethyl]-2,4,6-triethylbenzene (1030362-70-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / tetrahydrofuran; acetonitrile / 72 h / 20 °C

2: ammonia / water / 12 h

With ammonia; potassium carbonate; In tetrahydrofuran; water; acetonitrile;

DOI:10.1039/c0ob00960a

upstream raw materials:

2-Amino-4,6-dimethylpyridine

1,3,5-tris(bromomethyl)-2,4,6-triethylbenzene

Downstream raw materials:

1-[N-(1,10-phenanthrolin-2-ylcarbonyl)aminomethyl]-3,5-bis[(4,6-dimethylpyridin-2-yl)aminomethyl]-2,4,6-triethylbenzene

1-[(quinolin-2-ylmethyl)aminomethyl]-3,5-bis[(4,6-dimethylpyridin-2-yl)aminomethyl]-2,4,6-triethylbenzene

1-[(8-hydroxyquinolin-2-ylmethyl)aminomethyl]-3,5-bis[(4,6-dimethylpyridin-2-yl)aminomethyl]-2,4,6-triethylbenzene

C₁₄H₂₈O₆*C₃₉H₄₈N₆O