p-methoxyphenyl 3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranoside

Base Information

• Chemical Name: p-methoxyphenyl 3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranoside
• CAS No.: 1046460-97-2
• Molecular Formula: C₈₈H₉₂O₁₇
• Molecular Weight: 1421.69

Synonyms:p-methoxyphenyl 3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranoside

Chemical Property of p-methoxyphenyl 3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranoside

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Technology Process of p-methoxyphenyl 3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranoside

There total 1 articles about p-methoxyphenyl 3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

p-methoxyphenyl 2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranoside (1046460-96-1) → p-methoxyphenyl 3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranoside (1046460-97-2)

Guidance literature:

With sodium methylate; In methanol; dichloromethane; at 20 ℃; for 16h;

DOI:10.1016/j.carres.2008.02.025

Reference yield: 92.0%

2-O-benzoyl-3,4,6-tri-O-benzyl-D-mannopyranosyl trichloroacetimidate (1002744-50-4) + p-methoxyphenyl 3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranoside (1046460-97-2) → p-methoxyphenyl 2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h;

DOI:10.1016/j.carres.2008.02.025

Reference yield: 79.0%

2,4,6-tri-O-benzoyl-3-O-methyl-α-D-mannopyranosyl trichloroacetimidate (1046461-03-3) + p-methoxyphenyl 3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranoside (1046460-97-2) → p-methoxyphenyl 2,4,6-tri-O-benzoyl-3-O-methyl-α-D-mannopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranoside (1046461-05-5)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h;

DOI:10.1016/j.carres.2008.02.025

upstream raw materials:

p-methoxyphenyl 2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranoside

Downstream raw materials:

p-methoxyphenyl 2,4,6-tri-O-benzoyl-3-O-methyl-α-D-mannopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzyl-α-D-mannopyranoside

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