[(Pt(tri-n-butylphosphine)2(phenylethynyl))2Zn(5,15-bis(4-ethylphenyl)-10,20-bis(mesityl)porphyrinato^(4-))]

Base Information

• Chemical Name: [(Pt(tri-n-butylphosphine)2(phenylethynyl))2Zn(5,15-bis(4-ethylphenyl)-10,20-bis(mesityl)porphyrinato^(4-))]
• CAS No.: 1169873-74-8
• Molecular Formula: C₁₁₈H₁₅₆N₄P₄Pt₂Zn
• Molecular Weight: 2210.01

Synonyms:[(Pt(tri-n-butylphosphine)2(phenylethynyl))2Zn(5,15-bis(4-ethylphenyl)-10,20-bis(mesityl)porphyrinato^(4-))]

Chemical Property of [(Pt(tri-n-butylphosphine)2(phenylethynyl))2Zn(5,15-bis(4-ethylphenyl)-10,20-bis(mesityl)porphyrinato^(4-))]

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Technology Process of [(Pt(tri-n-butylphosphine)2(phenylethynyl))2Zn(5,15-bis(4-ethylphenyl)-10,20-bis(mesityl)porphyrinato^(4-))]

There total 1 articles about [(Pt(tri-n-butylphosphine)2(phenylethynyl))2Zn(5,15-bis(4-ethylphenyl)-10,20-bis(mesityl)porphyrinato^(4-))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.5%

5,15-bis(4-ethynylphenyl)-10,20-bis(mesityl)porphyrinatozinc(II) (247069-46-1) + trans-(chloro)(phenylacetylide)(tri-n-butylphosphine)platinum (II) (130269-70-4) → [(Pt(tri-n-butylphosphine)2(phenylethynyl))2Zn(5,15-bis(4-ethylphenyl)-10,20-bis(mesityl)porphyrinato(4-))] (1169873-74-8)

Guidance literature:

With HN(CH(CH₃)2)2; CuI; In dichloromethane; (N2, Schlenk technique); treatment of zinc compd. with 2 equiv. of platinum compd. in 1:1 mixt. of CH2Cl2 and diisopropylamine in presence of CuI for 12 h at 298 K; chromy. (silica gel, n-hexane/CH2Cl2 (2:3)), elem. anal.;

DOI:10.1021/ic900198h

upstream raw materials:

5,15-bis(4-ethynylphenyl)-10,20-bis(mesityl)porphyrinatozinc(II)

trans-(chloro)(phenylacetylide)(tri-n-butylphosphine)platinum (II)

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